Technology Process of C40H36O6
There total 7 articles about C40H36O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 20 ℃;
for 0.75h;
DOI:10.1039/c2cc30417a
- Guidance literature:
-
Multi-step reaction with 4 steps
1: copper(l) iodide; bis(benzonitrile)palladium(II) dichloride; triethylamine; triphenylphosphine / 6 h / 50 °C / Inert atmosphere
2: potassium carbonate / tetrahydrofuran; methanol / 19 h / 20 °C
3: copper(l) iodide; bis(benzonitrile)palladium(II) dichloride; tri-tert-butyl phosphine; triethylamine / 3 h / 50 °C / Inert atmosphere
4: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.75 h / 20 °C
With
copper(l) iodide; bis(benzonitrile)palladium(II) dichloride; tri-tert-butyl phosphine; tetrabutyl ammonium fluoride; potassium carbonate; triethylamine; triphenylphosphine;
In
tetrahydrofuran; methanol;
DOI:10.1039/c2cc30417a
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: hydrogenchloride; sodium nitrite / water / 0 °C
1.2: 1 h / 0 °C
2.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 3 h / Inert atmosphere
3.1: iodine; methyl iodide / 12 h / 100 °C / Inert atmosphere
4.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 1 h / 20 °C / Inert atmosphere
5.1: copper(l) iodide; bis(benzonitrile)palladium(II) dichloride; tri-tert-butyl phosphine; triethylamine / 3 h / 50 °C / Inert atmosphere
6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.75 h / 20 °C
With
hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; bis(benzonitrile)palladium(II) dichloride; tri-tert-butyl phosphine; tetrabutyl ammonium fluoride; iodine; triethylamine; sodium nitrite; methyl iodide;
In
tetrahydrofuran; water;
DOI:10.1039/c2cc30417a