(-)-N-<-2-naphthoyl>-L-phenylalanine-t-butyl ester

Base Information

Chemical Name:(-)-N-<-2-naphthoyl>-L-phenylalanine-t-butyl ester
CAS No.:149143-53-3
Molecular Formula:C₃₁H₃₁N₃O₄
Molecular Weight:509.605
Hs Code.:

(-)-N-<<N'-(3-aminobenzoyl)-5-amino>-2-naphthoyl>-L-phenylalanine-t-butyl ester

Synonyms:(-)-N-<-2-naphthoyl>-L-phenylalanine-t-butyl ester

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Chemical Property of (-)-N-<-2-naphthoyl>-L-phenylalanine-t-butyl ester

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Technology Process of (-)-N-<-2-naphthoyl>-L-phenylalanine-t-butyl ester

There total 6 articles about (-)-N-<-2-naphthoyl>-L-phenylalanine-t-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.8%

: 149143-52-2
(-)-N-<-2-naphthoyl>-L-phenylalanine-t-butyl ester

: 149143-53-3
(-)-N-<-2-naphthoyl>-L-phenylalanine-t-butyl ester

Guidance literature:: With hydrogen; Ra-Ni; In ethanol; ethyl acetate; for 0.833333h; under 1810.02 Torr;
DOI:10.1016/S0040-4020(01)90221-2

Reference yield:

: 149143-51-1
(-)-N-(5-amino-2-naphthoyl)-L-phenylalanine-t-butyl ester

: 149143-53-3
(-)-N-<-2-naphthoyl>-L-phenylalanine-t-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / tetrahydrofuran / a) 0.5 h, reflux, b) r.t., overnight

2: 77.8 percent / H₂ / Ra-Ni / ethyl acetate; ethanol / 0.83 h / 1810.02 Torr

With pyridine; hydrogen; Ra-Ni; In tetrahydrofuran; ethanol; ethyl acetate;
DOI:10.1016/S0040-4020(01)90221-2

Reference yield:

: 149143-49-7
(-)-N-(5-nitro-2-naphthoyl)-L-phenylalanine-t-butyl ester

: 149143-53-3
(-)-N-<-2-naphthoyl>-L-phenylalanine-t-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 94.4 percent / H₂ / Ra-Ni / ethyl acetate; ethanol / 0.75 h / 1810.02 Torr

2: pyridine / tetrahydrofuran / a) 0.5 h, reflux, b) r.t., overnight

3: 77.8 percent / H₂ / Ra-Ni / ethyl acetate; ethanol / 0.83 h / 1810.02 Torr

With pyridine; hydrogen; Ra-Ni; In tetrahydrofuran; ethanol; ethyl acetate;
DOI:10.1016/S0040-4020(01)90221-2