methyl 4-{[(2Z)-4-({4-chloro-2-[(diphenylmethyl)amino]benzoyl}amino)but-2-en-1-yl]oxy}benzoate

Base Information

• Chemical Name: methyl 4-{[(2Z)-4-({4-chloro-2-[(diphenylmethyl)amino]benzoyl}amino)but-2-en-1-yl]oxy}benzoate
• CAS No.: 1178873-68-1
• Molecular Formula: C₃₂H₂₉ClN₂O₄
• Molecular Weight: 541.046

Synonyms:methyl 4-{[(2Z)-4-({4-chloro-2-[(diphenylmethyl)amino]benzoyl}amino)but-2-en-1-yl]oxy}benzoate

Chemical Property of methyl 4-{[(2Z)-4-({4-chloro-2-[(diphenylmethyl)amino]benzoyl}amino)but-2-en-1-yl]oxy}benzoate

Chemical Property:

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Technology Process of methyl 4-{[(2Z)-4-({4-chloro-2-[(diphenylmethyl)amino]benzoyl}amino)but-2-en-1-yl]oxy}benzoate

There total 1 articles about methyl 4-{[(2Z)-4-({4-chloro-2-[(diphenylmethyl)amino]benzoyl}amino)but-2-en-1-yl]oxy}benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

methyl cis-4-(4-amino-but-2-enyloxy) benzoate (1178873-59-0) + 4-chloro-2-[(diphenylmethyl)amino]benzoic acid (1178873-58-9) → methyl 4-{[(2Z)-4-({4-chloro-2-[(diphenylmethyl)amino]benzoyl}amino)but-2-en-1-yl]oxy}benzoate (1178873-68-1)

Guidance literature:

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 5h;

DOI:10.1016/j.bmc.2009.05.027

Reference yield: 72.0%

bis(trichloromethyl) carbonate (32315-10-9) + methyl 4-{[(2Z)-4-({4-chloro-2-[(diphenylmethyl)amino]benzoyl}amino)but-2-en-1-yl]oxy}benzoate (1178873-68-1) → methyl 4-({(2Z)-4-[7-chloro-1-(diphenylmethyl)-2,4-dioxo-1,4-dihydroquinazolin-3(2H)-yl]but-2-en-1-yl}oxy)benzoate (1178873-75-0)

Guidance literature:

In tetrahydrofuran; for 20h; Reflux;

DOI:10.1016/j.bmc.2009.05.027

upstream raw materials:

methyl cis-4-(4-amino-but-2-enyloxy) benzoate

4-chloro-2-[(diphenylmethyl)amino]benzoic acid

Downstream raw materials:

methyl 4-({(2Z)-4-[7-chloro-1-(diphenylmethyl)-2,4-dioxo-1,4-dihydroquinazolin-3(2H)-yl]but-2-en-1-yl}oxy)benzoate

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