N²-<2-(4-nitrophenyl)ethoxycarbonyl>-O⁶-<2-(4-nitrophenyl)ethyl>guanosine

Base Information

• Chemical Name: N²-<2-(4-nitrophenyl)ethoxycarbonyl>-O⁶-<2-(4-nitrophenyl)ethyl>guanosine
• CAS No.: 148144-85-8
• Molecular Formula: C₂₇H₂₇N₇O₁₁
• Molecular Weight: 625.552

Synonyms:N²-<2-(4-nitrophenyl)ethoxycarbonyl>-O⁶-<2-(4-nitrophenyl)ethyl>guanosine

Chemical Property of N²-<2-(4-nitrophenyl)ethoxycarbonyl>-O⁶-<2-(4-nitrophenyl)ethyl>guanosine

Chemical Property:

Purity/Quality:

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• Hazard Codes: 

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Technology Process of N²-<2-(4-nitrophenyl)ethoxycarbonyl>-O⁶-<2-(4-nitrophenyl)ethyl>guanosine

There total 7 articles about N²-<2-(4-nitrophenyl)ethoxycarbonyl>-O⁶-<2-(4-nitrophenyl)ethyl>guanosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

2',3',5'-tri-O-acetyl-N2-<2-(4-nitrophenyl)ethoxycarbonyl>-O6-<2-(4-nitrophenyl)ethyl>guanosine → N2-<2-(4-nitrophenyl)ethoxycarbonyl>-O6-<2-(4-nitrophenyl)ethyl>guanosine (148144-85-8)

Guidance literature:

With ammonium hydroxide; In 1,4-dioxane; methanol; water; at 8 ℃; for 20h;

DOI:10.1002/hlca.19950780706

Reference yield:

2-(4-nitrophenyl)ethanol (100-27-6) → N2-<2-(4-nitrophenyl)ethoxycarbonyl>-O6-<2-(4-nitrophenyl)ethyl>guanosine (148144-85-8)

Guidance literature:

Multi-step reaction with 3 steps

1: PPh₃, diethyl azodicarboxylate / dioxane / 1 h / 60 °C

2: pyridine / CH₂Cl₂ / 18 h / Ambient temperature

3: 48 percent / 25 percent NH₃ / H₂O; methanol; dioxane / 20 h / 8 °C

With pyridine; ammonium hydroxide; triphenylphosphine; diethylazodicarboxylate; In 1,4-dioxane; methanol; dichloromethane; water;

DOI:10.1002/hlca.19950780706

Reference yield:

2',3',5'-tri-O-acetylguanosine (6979-94-8) → N2-<2-(4-nitrophenyl)ethoxycarbonyl>-O6-<2-(4-nitrophenyl)ethyl>guanosine (148144-85-8)

Guidance literature:

Multi-step reaction with 3 steps

1: PPh₃, diethyl azodicarboxylate / dioxane / 1 h / 60 °C

2: pyridine / CH₂Cl₂ / 18 h / Ambient temperature

3: 48 percent / 25 percent NH₃ / H₂O; methanol; dioxane / 20 h / 8 °C

With pyridine; ammonium hydroxide; triphenylphosphine; diethylazodicarboxylate; In 1,4-dioxane; methanol; dichloromethane; water;

DOI:10.1002/hlca.19950780706

upstream raw materials:

2',3',5'-tri-O-acetylguanosine

2-(4-nitrophenyl)ethanol

2',3',5'-tri-O-acetyl-O⁶-<2-(4-nitrophenyl)ethyl>guanosine

2′,3′,5′-tri-O-acetyl-O⁶-[2-(4-nitrophenyl)ethyl]guanosine

Downstream raw materials:

N²-<2-(4-nitrophenyl)ethoxycarbonyl>-O⁶-<2-(4-nitrophenyl)ethyl>-9-<3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl>guanine

5'-O-(monomethoxytrityl)-N²-<2-(4-nitrophenyl)ethoxycarbonyl>-O⁶-<2-(4-nitrophenyl)ethyl>guanosine

5'-O-(dimethoxytrityl)-N²-<2-(4-nitrophenyl)ethoxycarbonyl>-O⁶-<2-(4-nitrophenyl)ethyl>guanosine

N²-{[2-(4-nitrophenyl)ethoxy]carbonyl}-O⁶-[2-(4-nitrophenyl)ethyl]-2'-O-(tetrahydro-4-methoxy-2H-pyran-4-yl)guanosine

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