trans N(meta-trifluoromethylphenyl) (chloro-2' biphenylyl-4)-4 methyl-2 oxo-4 butene-2 amide

Base Information

Chemical Name:trans N(meta-trifluoromethylphenyl) (chloro-2' biphenylyl-4)-4 methyl-2 oxo-4 butene-2 amide
CAS No.:111259-52-0
Molecular Formula:C₂₄H₁₇ClF₃NO₂
Molecular Weight:443.853
Hs Code.:

Synonyms:trans N(meta-trifluoromethylphenyl) (chloro-2' biphenylyl-4)-4 methyl-2 oxo-4 butene-2 amide

Suppliers and Price of trans N(meta-trifluoromethylphenyl) (chloro-2' biphenylyl-4)-4 methyl-2 oxo-4 butene-2 amide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of trans N(meta-trifluoromethylphenyl) (chloro-2' biphenylyl-4)-4 methyl-2 oxo-4 butene-2 amide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of trans N(meta-trifluoromethylphenyl) (chloro-2' biphenylyl-4)-4 methyl-2 oxo-4 butene-2 amide

There total 4 articles about trans N(meta-trifluoromethylphenyl) (chloro-2' biphenylyl-4)-4 methyl-2 oxo-4 butene-2 amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 98-16-8
3-trifluoromethylaniline

: 111259-50-8
chlorure de trans (chloro-2' biphenylyl-4)-4 methyl-2 oxo-4 butene-2 oyle

: 111259-52-0
trans N(meta-trifluoromethylphenyl) (chloro-2' biphenylyl-4)-4 methyl-2 oxo-4 butene-2 amide

Guidance literature:: With pyridine; In benzene; R_.T_., overnight then 50 deg C, 2 h 30 min;
DOI:10.1016/0223-5234(87)90173-5

Reference yield:

: 2051-60-7,108321-69-3
2-chloro-1,1'-biphenyl

: 111259-52-0
trans N(meta-trifluoromethylphenyl) (chloro-2' biphenylyl-4)-4 methyl-2 oxo-4 butene-2 amide

Guidance literature:: Multi-step reaction with 4 steps

1: 62 percent / anhydr. aluminum chloride / CH₂Cl₂ / 3 h / 35 - 40 °C

2: 70 percent / triethylamine / H₂O / 12 h / Ambient temperature

3: 74 percent / phosphorous pentachloride / cyclohexane / 0.67 h / Heating

4: 56 percent / pyridine / benzene / R_.T_., overnight then 50 deg C, 2 h 30 min

With pyridine; aluminium trichloride; phosphorus pentachloride; triethylamine; In dichloromethane; cyclohexane; water; benzene;
DOI:10.1016/0223-5234(87)90173-5

Reference yield:

: 73844-65-2
4-<4'-(2-chlorophenyl)phenyl>-4-oxo-2-methyl-2-butenoic acid

: 111259-52-0
trans N(meta-trifluoromethylphenyl) (chloro-2' biphenylyl-4)-4 methyl-2 oxo-4 butene-2 amide

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / phosphorous pentachloride / cyclohexane / 0.67 h / Heating

2: 56 percent / pyridine / benzene / R_.T_., overnight then 50 deg C, 2 h 30 min

With pyridine; phosphorus pentachloride; In cyclohexane; benzene;
DOI:10.1016/0223-5234(87)90173-5