6-methoxy-2-(p-methoxyphenyl)-2-methyl-1,2,3,4-tetrahydronaphthalen-1ζ-ol

Base Information

Chemical Name:6-methoxy-2-(p-methoxyphenyl)-2-methyl-1,2,3,4-tetrahydronaphthalen-1ζ-ol
CAS No.:96043-75-3
Molecular Formula:C₁₉H₂₂O₃
Molecular Weight:298.382
Hs Code.:

Synonyms:6-methoxy-2-(p-methoxyphenyl)-2-methyl-1,2,3,4-tetrahydronaphthalen-1ζ-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-methoxy-2-(p-methoxyphenyl)-2-methyl-1,2,3,4-tetrahydronaphthalen-1ζ-ol

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Technology Process of 6-methoxy-2-(p-methoxyphenyl)-2-methyl-1,2,3,4-tetrahydronaphthalen-1ζ-ol

There total 8 articles about 6-methoxy-2-(p-methoxyphenyl)-2-methyl-1,2,3,4-tetrahydronaphthalen-1ζ-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 96034-07-0
6-methoxy-2-(p-methoxyphenyl)-2-methyl-3,4-dihydronaphthalen-1(2H)-one

: 96043-75-3
6-methoxy-2-(p-methoxyphenyl)-2-methyl-1,2,3,4-tetrahydronaphthalen-1ζ-ol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; for 15h; Heating;
DOI:10.1071/CH9842279

Reference yield:

: 2-[1-Benzyloxy-meth-(E)-ylidene]-6-methoxy-3,4-dihydro-2H-naphthalen-1-one

: 96043-75-3
6-methoxy-2-(p-methoxyphenyl)-2-methyl-1,2,3,4-tetrahydronaphthalen-1ζ-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / H₂, TEA / PtO / propan-2-ol / 760 Torr / Ambient temperature

2: 99 percent / sulfuryl chloride / CCl₄ / 12 h / Ambient temperature

3: 25 percent / tetrahydrofuran; benzene / 3 h / Heating

4: 99 percent / LiAlH₄ / diethyl ether / 15 h / Heating

With lithium aluminium tetrahydride; sulfuryl dichloride; TEA; hydrogen; platinum(II) oxide; In tetrahydrofuran; tetrachloromethane; diethyl ether; isopropyl alcohol; benzene;
DOI:10.1071/CH9842279

Reference yield:

: 27752-24-5,888007-82-7,1129429-21-5,745033-23-2
6-methoxy-2-methyl-3,4-dihydronaphthalen-1(2H)-one

: 96043-75-3
6-methoxy-2-(p-methoxyphenyl)-2-methyl-1,2,3,4-tetrahydronaphthalen-1ζ-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / sulfuryl chloride / CCl₄ / 12 h / Ambient temperature

2: 25 percent / tetrahydrofuran; benzene / 3 h / Heating

3: 99 percent / LiAlH₄ / diethyl ether / 15 h / Heating

With lithium aluminium tetrahydride; sulfuryl dichloride; In tetrahydrofuran; tetrachloromethane; diethyl ether; benzene;
DOI:10.1071/CH9842279