9-(4-(3'-bromobenzylamino)butyl)-9-azabicyclo[3.3.1]nonan-3α-yl 2-methoxy-5-methylphenylcarbamate

Base Information

Chemical Name:9-(4-(3'-bromobenzylamino)butyl)-9-azabicyclo[3.3.1]nonan-3α-yl 2-methoxy-5-methylphenylcarbamate
CAS No.:913815-85-7
Molecular Formula:C₂₈H₃₈BrN₃O₃
Molecular Weight:544.532
Hs Code.:

Synonyms:9-(4-(3'-bromobenzylamino)butyl)-9-azabicyclo[3.3.1]nonan-3α-yl 2-methoxy-5-methylphenylcarbamate

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Chemical Property of 9-(4-(3'-bromobenzylamino)butyl)-9-azabicyclo[3.3.1]nonan-3α-yl 2-methoxy-5-methylphenylcarbamate

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Technology Process of 9-(4-(3'-bromobenzylamino)butyl)-9-azabicyclo[3.3.1]nonan-3α-yl 2-methoxy-5-methylphenylcarbamate

There total 4 articles about 9-(4-(3'-bromobenzylamino)butyl)-9-azabicyclo[3.3.1]nonan-3α-yl 2-methoxy-5-methylphenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: (2-Methoxy-5-methyl-phenyl)-carbamic acid (1R,3R,5S)-9-(4-{[1-(3-bromo-phenyl)-meth-(E)-ylidene]-amino}-butyl)-9-aza-bicyclo[3.3.1]non-3-yl ester

: 913815-85-7
9-(4-(3'-bromobenzylamino)butyl)-9-azabicyclo[3.3.1]nonan-3α-yl 2-methoxy-5-methylphenylcarbamate

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 20 ℃;
DOI:10.1016/j.bmc.2006.06.028

Reference yield:

: 371226-28-7
O-(9-azabicyclo[3.3.1]nonan-3α-yl)-N-(2-methoxy-5-methylphenyl)carbamate

: 913815-85-7
9-(4-(3'-bromobenzylamino)butyl)-9-azabicyclo[3.3.1]nonan-3α-yl 2-methoxy-5-methylphenylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1: K₂CO₃; KI / acetonitrile / Heating

2: hydrazine hydrate / ethanol / 2 h / Heating

3: 100 percent / benzene / 2 h / 90 °C

4: 100 percent / sodium borohydride / ethanol / 20 °C

With sodium tetrahydroborate; potassium carbonate; hydrazine hydrate; potassium iodide; In ethanol; acetonitrile; benzene;
DOI:10.1016/j.bmc.2006.06.028

Reference yield:

: 913815-80-2
9-(4-aminobutyl)-9-azabicyclo[3.3.1]nonan-3α-yl 2-methoxy-5-methylphenylcarbamate

: 913815-85-7
9-(4-(3'-bromobenzylamino)butyl)-9-azabicyclo[3.3.1]nonan-3α-yl 2-methoxy-5-methylphenylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / benzene / 2 h / 90 °C

2: 100 percent / sodium borohydride / ethanol / 20 °C

With sodium tetrahydroborate; In ethanol; benzene;
DOI:10.1016/j.bmc.2006.06.028