(2S,3R,2'S,3'R)-3,3'-Bis-(tert-butyl-diphenyl-silanyloxymethyl)-[2,2']bioxiranyl

Base Information

Chemical Name:(2S,3R,2'S,3'R)-3,3'-Bis-(tert-butyl-diphenyl-silanyloxymethyl)-[2,2']bioxiranyl
CAS No.:129966-01-4
Molecular Formula:C₃₈H₄₆O₄Si₂
Molecular Weight:622.952
Hs Code.:

Synonyms:(2S,3R,2'S,3'R)-3,3'-Bis-(tert-butyl-diphenyl-silanyloxymethyl)-[2,2']bioxiranyl

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3R,2'S,3'R)-3,3'-Bis-(tert-butyl-diphenyl-silanyloxymethyl)-[2,2']bioxiranyl

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Technology Process of (2S,3R,2'S,3'R)-3,3'-Bis-(tert-butyl-diphenyl-silanyloxymethyl)-[2,2']bioxiranyl

There total 2 articles about (2S,3R,2'S,3'R)-3,3'-Bis-(tert-butyl-diphenyl-silanyloxymethyl)-[2,2']bioxiranyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 20706-76-7
(2S,3R,2'S,3'R)-3'-hydroxymethyl-([2,2]bioxiranyl-3-yl)methanol

: 58479-61-1
tert-butylchlorodiphenylsilane

: 129966-01-4
(2S,3R,2'S,3'R)-3,3'-Bis-(tert-butyl-diphenyl-silanyloxymethyl)-[2,2']bioxiranyl

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 22 ℃; for 12h;

Reference yield:

: 20706-73-4
3,4-di-O-p-toluenesulfonyl-D-mannitol

: 129966-01-4
(2S,3R,2'S,3'R)-3,3'-Bis-(tert-butyl-diphenyl-silanyloxymethyl)-[2,2']bioxiranyl

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / K₂CO₃ / methanol / 3 h / 22 °C

2: 95 percent / Imidazol / dimethylformamide / 12 h / 22 °C

With 1H-imidazole; potassium carbonate; In methanol; N,N-dimethyl-formamide;