3-(6-cyclopropanesulfonylpyridin-3-yloxy)-5-isobutylbenzoic acid methyl ester

Base Information

Chemical Name:3-(6-cyclopropanesulfonylpyridin-3-yloxy)-5-isobutylbenzoic acid methyl ester
CAS No.:1325708-49-3
Molecular Formula:C₂₀H₂₃NO₅S
Molecular Weight:389.472
Hs Code.:

Synonyms:3-(6-cyclopropanesulfonylpyridin-3-yloxy)-5-isobutylbenzoic acid methyl ester

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Chemical Property of 3-(6-cyclopropanesulfonylpyridin-3-yloxy)-5-isobutylbenzoic acid methyl ester

Chemical Property:

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Technology Process of 3-(6-cyclopropanesulfonylpyridin-3-yloxy)-5-isobutylbenzoic acid methyl ester

There total 8 articles about 3-(6-cyclopropanesulfonylpyridin-3-yloxy)-5-isobutylbenzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1119778-92-5
3-hydroxy-5-isobutylbenzoic acid methyl ester

: 1177422-05-7
5-Chloro-2-(cyclopropylsulfonyl)pyridine

: 1325708-49-3
3-(6-cyclopropanesulfonylpyridin-3-yloxy)-5-isobutylbenzoic acid methyl ester

Guidance literature:: With caesium carbonate; In ISOPROPYLAMIDE; at 100 ℃; for 6h;

Reference yield:

: 1119778-91-4
3-benzyloxy-5-isobutylbenzoic acid methyl ester

: 1325708-49-3
3-(6-cyclopropanesulfonylpyridin-3-yloxy)-5-isobutylbenzoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylsilane / palladium 10% on activated carbon / ethanol / 20 °C / Inert atmosphere

2: caesium carbonate / ISOPROPYLAMIDE / 6 h / 100 °C

With triethylsilane; caesium carbonate; palladium 10% on activated carbon; In ethanol; ISOPROPYLAMIDE;

Reference yield:

: 168619-23-6
methyl 3-benzyloxy-5-{[trifluoromethylsulfonyl]oxy}benzoate

: 1325708-49-3
3-(6-cyclopropanesulfonylpyridin-3-yloxy)-5-isobutylbenzoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: lithium chloride / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / Inert atmosphere; Reflux

2: triethylsilane / palladium 10% on activated carbon / ethanol / 20 °C / Inert atmosphere

3: caesium carbonate / ISOPROPYLAMIDE / 6 h / 100 °C

With triethylsilane; caesium carbonate; lithium chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; ISOPROPYLAMIDE;