(Z,Z)-cycloocta-1,5-diene(1,4-bis(dicyclohexylphosphino)butane)rhodium(I) tetrafluoroborate

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Chemical Name:(Z,Z)-cycloocta-1,5-diene(1,4-bis(dicyclohexylphosphino)butane)rhodium(I) tetrafluoroborate
CAS No.:255064-34-7
Molecular Formula:BF₄*C₃₆H₆₄P₂Rh
Molecular Weight:748.562
Hs Code.:

Synonyms:(Z,Z)-cycloocta-1,5-diene(1,4-bis(dicyclohexylphosphino)butane)rhodium(I) tetrafluoroborate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z,Z)-cycloocta-1,5-diene(1,4-bis(dicyclohexylphosphino)butane)rhodium(I) tetrafluoroborate

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Technology Process of (Z,Z)-cycloocta-1,5-diene(1,4-bis(dicyclohexylphosphino)butane)rhodium(I) tetrafluoroborate

There total 1 articles about (Z,Z)-cycloocta-1,5-diene(1,4-bis(dicyclohexylphosphino)butane)rhodium(I) tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: tetrafluoroboric acid

: acethylacetonato(1,5-cyclooctadiene)rhodium(I)

: 65038-36-0
1,4-bis(dicyclohexylphosphino)butane

: 255064-34-7
(Z,Z)-cycloocta-1,5-diene(1,4-bis(dicyclohexylphosphino)butane)rhodium(I) tetrafluoroborate

Guidance literature:: In tetrahydrofuran; stirred soln. of ligand and Rh complex (molar ratio 1:1) in abs. THF treated at room temp. with aq. HBF4; stirred for 20 min; diluted with abs. Et2O; solvent removed by tube filtration; washed with Et2O; solid dried under reduced pressure; recrystd. from CHCl3-hexane;
DOI:10.1016/S0022-328X(00)00845-7