benzyl (2S,5R)-3-aza-8-(1,1-dimethylethoxycarbonylamino)-5-(9H-9-fluorenylmethoxycarboxamido)-2-(2-methylpropyl)-4-oxooctanoate

Base Information

Chemical Name:benzyl (2S,5R)-3-aza-8-(1,1-dimethylethoxycarbonylamino)-5-(9H-9-fluorenylmethoxycarboxamido)-2-(2-methylpropyl)-4-oxooctanoate
CAS No.:1233399-01-3
Molecular Formula:C₃₈H₄₇N₃O₇
Molecular Weight:657.807
Hs Code.:

Synonyms:benzyl (2S,5R)-3-aza-8-(1,1-dimethylethoxycarbonylamino)-5-(9H-9-fluorenylmethoxycarboxamido)-2-(2-methylpropyl)-4-oxooctanoate

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Chemical Property of benzyl (2S,5R)-3-aza-8-(1,1-dimethylethoxycarbonylamino)-5-(9H-9-fluorenylmethoxycarboxamido)-2-(2-methylpropyl)-4-oxooctanoate

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Technology Process of benzyl (2S,5R)-3-aza-8-(1,1-dimethylethoxycarbonylamino)-5-(9H-9-fluorenylmethoxycarboxamido)-2-(2-methylpropyl)-4-oxooctanoate

There total 1 articles about benzyl (2S,5R)-3-aza-8-(1,1-dimethylethoxycarbonylamino)-5-(9H-9-fluorenylmethoxycarboxamido)-2-(2-methylpropyl)-4-oxooctanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 2462-35-3
L-leucine benzyl ester hydrochloride

: 118476-89-4
(R)-N₅-(tert.-butoxy-carbonyl)-N₂-(9-fluorenylmethoxycarbonyl)-ornithine

: 1233399-01-3
benzyl (2S,5R)-3-aza-8-(1,1-dimethylethoxycarbonylamino)-5-(9H-9-fluorenylmethoxycarboxamido)-2-(2-methylpropyl)-4-oxooctanoate

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In acetonitrile; at 20 ℃;
DOI:10.1016/j.bmc.2010.02.033

Reference yield: 94.0%

: 1233399-01-3
benzyl (2S,5R)-3-aza-8-(1,1-dimethylethoxycarbonylamino)-5-(9H-9-fluorenylmethoxycarboxamido)-2-(2-methylpropyl)-4-oxooctanoate

: C₃₃H₃₉N₃O₅*ClH

Guidance literature:: benzyl (2S,5R)-3-aza-8-(1,1-dimethylethoxycarbonylamino)-5-(9H-9-fluorenylmethoxycarboxamido)-2-(2-methylpropyl)-4-oxooctanoate; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h;

With hydrogenchloride; In diethyl ether;
DOI:10.1016/j.bmc.2010.02.033