C₃₂H₄₀O₇

Base Information

Chemical Name:C₃₂H₄₀O₇
CAS No.:391278-03-8
Molecular Formula:C₃₂H₄₀O₇
Molecular Weight:536.665
Hs Code.:

C<sub>32</sub>H<sub>40</sub>O<sub>7</sub>

Synonyms:C₃₂H₄₀O₇

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Chemical Property of C₃₂H₄₀O₇

Chemical Property:

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Technology Process of C₃₂H₄₀O₇

There total 20 articles about C₃₂H₄₀O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 391278-15-2
C₃₃H₄₄O₈

: 391278-03-8
C₃₂H₄₀O₇

Guidance literature:: With sodium periodate;
DOI:10.1016/S0040-4039(01)01802-0

Reference yield: 78.0%

: 391278-02-7
C₃₃H₄₂O₆

: 391278-03-8
C₃₂H₄₀O₇

Guidance literature:: C₃₃H₄₂O₆; With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In water; acetone; at 20 ℃; for 96h;

With sodium periodate; In water; acetone; at 20 ℃; for 48h;
DOI:10.1016/j.tet.2004.07.094

Reference yield:

: 2244-16-8,6485-40-1
(S)-p-mentha-6,8-dien-2-one

: 391278-03-8
C₃₂H₄₀O₇

Guidance literature:: Multi-step reaction with 12 steps

1.1: 92 percent / EtAlCl₂ / toluene; hexane / 28 h / 20 °C

2.1: 89 percent / p-TsOH / benzene / 12 h / Heating

3.1: N-methylmorpholine-N-oxide; OsO₄ / acetone; H₂O / 216 h / 20 °C

3.2: 74 percent / NaIO₄ / acetone; H₂O / 1 h / 20 °C

4.1: 93 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 72 h / 20 °C

5.1: 92 percent / p-TsOH / CH₂Cl₂ / 24 h / 20 °C

6.1: K₂CO₃ / methanol / 4 h / 20 °C

6.2: 90 percent / PCC / CH₂Cl₂ / 3 h / 20 °C

7.1: 88 percent / Et₃N / CH₂Cl₂ / 0.5 h / -78 °C

8.1: 73 percent / Na₂(EDTA); oxone; NaHCO₃ / H₂O; acetone; acetonitrile / 4 h / 20 °C

9.1: 79 percent / Al(OiPr)3 / toluene / 1 h / 20 °C

10.1: Me₃SiCl; Et₃N; DMAP / CH₂Cl₂ / 0.33 h / 20 °C

10.2: tetrahydrofuran / 0.17 h / -78 °C

10.3: 90 percent / HCl / tetrahydrofuran; H₂O / 0.5 h / 20 °C

11.1: NaH / tetrahydrofuran / 0 - 20 °C

11.2: 86 percent / tetrahydrofuran / 12 h / Heating

12.1: OsO₄; N-methylmorpholine-N-oxide / acetone; H₂O / 96 h / 20 °C

12.2: 78 percent / NaIO₄ / acetone; H₂O / 48 h / 20 °C

With dmap; Oxone; osmium(VIII) oxide; chloro-trimethyl-silane; ethylaluminum dichloride; edetate disodium; aluminum isopropoxide; sodium hydride; sodium hydrogencarbonate; potassium carbonate; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; hexane; dichloromethane; water; acetone; toluene; acetonitrile; benzene; 1.1: Diels-Alder reaction / 4.1: Baeyer-Villiger oxidation;
DOI:10.1016/j.tet.2004.07.094