methyl 3α,7β-diacetoxy-5β-cholan-24-oate-11,12-d2

Base Information

• Chemical Name: methyl 3α,7β-diacetoxy-5β-cholan-24-oate-11,12-d2
• CAS No.: 77285-16-6
• Molecular Formula: C₂₉H₄₆O₆
• Molecular Weight: 492.665

Synonyms:methyl 3α,7β-diacetoxy-5β-cholan-24-oate-11,12-d2

Chemical Property of methyl 3α,7β-diacetoxy-5β-cholan-24-oate-11,12-d2

Chemical Property:

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Technology Process of methyl 3α,7β-diacetoxy-5β-cholan-24-oate-11,12-d2

There total 1 articles about methyl 3α,7β-diacetoxy-5β-cholan-24-oate-11,12-d2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

7-ketodeoxycholic acid (911-40-0) → methyl 3α,7β-diacetoxy-5β-cholan-24-oate-11,12-d2 (77285-16-6)

Guidance literature:

Multi-step reaction with 6 steps

1: Na / propan-1-ol

2: 14.0 g / HCl / 1.5 h / Heating

3: 5.7 g / pyridine / benzene / Ambient temperature

4: 6.0 g / pyridine / 48 h / 0 °C

5: 3.0 g / NaOAc / hexamethylphosphoric acid triamide / 28 h / 100 °C

6: 1.35 g / D₂, DClO₄ / PtO₂ / dioxane / 48 h / 3677.5 Torr

With pyridine; hydrogenchloride; sodium acetate; deuteroperchloric acid; sodium; deuterium; platinum(IV) oxide; In 1,4-dioxane; propan-1-ol; N,N,N,N,N,N-hexamethylphosphoric triamide; benzene;

DOI:10.1248/cpb.29.137

upstream raw materials:

7-ketodeoxycholic acid

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