HCC(OH)C(Ph)-CC-(Ph)C(OH)CCH

Base Information

Chemical Name:HCC(OH)C(Ph)-CC-(Ph)C(OH)CCH
CAS No.:864519-29-9
Molecular Formula:C₂₀H₁₄O₂
Molecular Weight:286.33
Hs Code.:

Synonyms:HCC(OH)C(Ph)-CC-(Ph)C(OH)CCH

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Chemical Property of HCC(OH)C(Ph)-CC-(Ph)C(OH)CCH

Chemical Property:

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Technology Process of HCC(OH)C(Ph)-CC-(Ph)C(OH)CCH

There total 3 articles about HCC(OH)C(Ph)-CC-(Ph)C(OH)CCH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1087-09-8
1,4-diphenyl-but-2-yne-1,4-dione

: 74-86-2,25067-58-7
acetylene

: 864519-29-9
HCC(OH)C(Ph)-CC-(Ph)C(OH)CCH

Guidance literature:: acetylene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

1,4-diphenyl-but-2-yne-1,4-dione; In tetrahydrofuran; hexane; at 20 ℃;
DOI:10.1002/ejic.200400457

Reference yield: 79.0%

: 1,8-bis(trimethylsilyl)-3,6-diphenylocta-1,4,7-triyne-3,6-diol

: 864519-29-9
HCC(OH)C(Ph)-CC-(Ph)C(OH)CCH

Guidance literature:: With methanol; potassium carbonate; Inert atmosphere;
DOI:10.1002/chem.201002769

Reference yield:

: 1087-09-8
1,4-diphenyl-but-2-yne-1,4-dione

: 864519-29-9
HCC(OH)C(Ph)-CC-(Ph)C(OH)CCH

Guidance literature:: Multi-step reaction with 2 steps

1.1: Inert atmosphere

1.2: Inert atmosphere

2.1: methanol; potassium carbonate / Inert atmosphere

With methanol; potassium carbonate;
DOI:10.1002/chem.201002769