C₆₇H₁₁₃O₁₃Si₂N

Base Information

Chemical Name:C₆₇H₁₁₃O₁₃Si₂N
CAS No.:930803-58-0
Molecular Formula:C₆₇H₁₁₃NO₁₃Si₂
Molecular Weight:1196.8
Hs Code.:

C<sub>67</sub>H<sub>113</sub>O<sub>13</sub>Si<sub>2</sub>N

Synonyms:C₆₇H₁₁₃O₁₃Si₂N

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Chemical Property of C₆₇H₁₁₃O₁₃Si₂N

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Technology Process of C₆₇H₁₁₃O₁₃Si₂N

There total 17 articles about C₆₇H₁₁₃O₁₃Si₂N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 930803-57-9
C₅₆H₉₆O₁₀Si₂

: 26250-84-0
(S)-(-)-1-(tert-butoxycarbonyl)-2-piperidinecarboxylic acid

: 930803-58-0
C₆₇H₁₁₃O₁₃Si₂N

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at -5 ℃; for 24h;
DOI:10.1002/anie.200604053

Reference yield:

: 930803-26-2
C₉H₁₅S₂OBr

: 930803-58-0
C₆₇H₁₁₃O₁₃Si₂N

Guidance literature:: Multi-step reaction with 7 steps

1: 70 percent / methanesulfonyl chloride; triethylamine; 4-(dimethylamino)pyridine / lithium bromide / CH₂Cl₂; dimethylformamide

2: 99 percent / LiBHEt₃ / tetrahydrofuran / 0 °C

3: tert-butyllithium / tetrahydrofuran / -96 - -78 °C

4: 99 percent / 2,6-lutidine / CH₂Cl₂ / 0.67 h / -78 °C

5: 77 percent / tert-butyllithium; hexamethylphosphoramide / tetrahydrofuran / -78 - -40 °C

6: 84 percent / (bis(trifluoroacetoxy)iodo)benzene / tetrahydrofuran; H₂O; methanol / 20 °C

7: 84 percent / 1,3-dicyclohexylcarbodiimide; 4-(dimethylamino)pyridine / CH₂Cl₂ / 24 h / -5 °C

With 2,6-dimethylpyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; tert.-butyl lithium; lithium triethylborohydride; methanesulfonyl chloride; triethylamine; dicyclohexyl-carbodiimide; bis-[(trifluoroacetoxy)iodo]benzene; lithium bromide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/anie.200604053

Reference yield:

: 930803-25-1
C₁₀H₁₅S₂O₂Br

: 930803-58-0
C₆₇H₁₁₃O₁₃Si₂N

Guidance literature:: Multi-step reaction with 8 steps

1: 99 percent / diisobutylaluminum hydride / CH₂Cl₂ / -45 °C

2: 70 percent / methanesulfonyl chloride; triethylamine; 4-(dimethylamino)pyridine / lithium bromide / CH₂Cl₂; dimethylformamide

3: 99 percent / LiBHEt₃ / tetrahydrofuran / 0 °C

4: tert-butyllithium / tetrahydrofuran / -96 - -78 °C

5: 99 percent / 2,6-lutidine / CH₂Cl₂ / 0.67 h / -78 °C

6: 77 percent / tert-butyllithium; hexamethylphosphoramide / tetrahydrofuran / -78 - -40 °C

7: 84 percent / (bis(trifluoroacetoxy)iodo)benzene / tetrahydrofuran; H₂O; methanol / 20 °C

8: 84 percent / 1,3-dicyclohexylcarbodiimide; 4-(dimethylamino)pyridine / CH₂Cl₂ / 24 h / -5 °C

With 2,6-dimethylpyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; tert.-butyl lithium; diisobutylaluminium hydride; lithium triethylborohydride; methanesulfonyl chloride; triethylamine; dicyclohexyl-carbodiimide; bis-[(trifluoroacetoxy)iodo]benzene; lithium bromide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/anie.200604053