5'-O-(tert-butyldiphenylsilyl)-2'-amino>-2'-deoxyuridine

Base Information

Chemical Name:5'-O-(tert-butyldiphenylsilyl)-2'-amino>-2'-deoxyuridine
CAS No.:219618-70-9
Molecular Formula:C₃₀H₃₈N₄O₈Si
Molecular Weight:610.739
Hs Code.:

5'-O-(tert-butyldiphenylsilyl)-2'-<N-carbamoyl-N-<(2-tetrahydrofuranyl)oxy>amino>-2'-deoxyuridine

Synonyms:5'-O-(tert-butyldiphenylsilyl)-2'-amino>-2'-deoxyuridine

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Chemical Property of 5'-O-(tert-butyldiphenylsilyl)-2'-amino>-2'-deoxyuridine

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Technology Process of 5'-O-(tert-butyldiphenylsilyl)-2'-amino>-2'-deoxyuridine

There total 3 articles about 5'-O-(tert-butyldiphenylsilyl)-2'-amino>-2'-deoxyuridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 175013-53-3
2'-(benzyloxyamino)-5'-O-(tert-butyldiphenylsilyl)-2'-N,3'-O-carbonyl-2'-deoxyuridine

: 219618-70-9
5'-O-(tert-butyldiphenylsilyl)-2'-amino>-2'-deoxyuridine

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / H₂ / 10 percent Pd/C / ethanol / 24 h / Ambient temperature

2: 100 percent / PPTS / tetrahydrofuran / 11 h / Ambient temperature

3: 28 percent aq. NH₄OH / dioxane / 24 h / Ambient temperature

With ammonium hydroxide; hydrogen; pyridinium p-toluenesulfonate; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; ethanol;
DOI:10.1021/jm980466g

Reference yield:

: 214055-25-1
5'-O-(tert-butyldiphenylsilyl)-2'-N,3'-O-carbonyl-2'-deoxy-2'-<(2-tetrahydrofuranyl)oxyamino>uridine

: 219618-70-9
5'-O-(tert-butyldiphenylsilyl)-2'-amino>-2'-deoxyuridine

Guidance literature:: With ammonium hydroxide; In 1,4-dioxane; for 24h; Ambient temperature;
DOI:10.1021/jm980466g

Reference yield:

: 175013-49-7
5'-O-(tert-butyldiphenylsilyl)-2'-N,3'-O-carbonyl-2'-deoxy-2'-(hydroxylamino)uridine

: 219618-70-9
5'-O-(tert-butyldiphenylsilyl)-2'-amino>-2'-deoxyuridine

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / PPTS / tetrahydrofuran / 11 h / Ambient temperature

2: 28 percent aq. NH₄OH / dioxane / 24 h / Ambient temperature

With ammonium hydroxide; pyridinium p-toluenesulfonate; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1021/jm980466g