4,4'-(2,2'-dihydroxybiphenyl-3,3'-diyl)bis(N₂,N₆-bis(2-((S)-4-methyl-4,5-dihydrooxazol-2-yl)phenyl)pyridine-2,6-dicarboxamide)

Base Information

• Chemical Name: 4,4'-(2,2'-dihydroxybiphenyl-3,3'-diyl)bis(N₂,N₆-bis(2-((S)-4-methyl-4,5-dihydrooxazol-2-yl)phenyl)pyridine-2,6-dicarboxamide)
• CAS No.: 1037078-43-5
• Molecular Formula: C₆₆H₅₆N₁₀O₁₀
• Molecular Weight: 1149.23

Synonyms:4,4'-(2,2'-dihydroxybiphenyl-3,3'-diyl)bis(N₂,N₆-bis(2-((S)-4-methyl-4,5-dihydrooxazol-2-yl)phenyl)pyridine-2,6-dicarboxamide)

Chemical Property of 4,4'-(2,2'-dihydroxybiphenyl-3,3'-diyl)bis(N₂,N₆-bis(2-((S)-4-methyl-4,5-dihydrooxazol-2-yl)phenyl)pyridine-2,6-dicarboxamide)

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Technology Process of 4,4'-(2,2'-dihydroxybiphenyl-3,3'-diyl)bis(N₂,N₆-bis(2-((S)-4-methyl-4,5-dihydrooxazol-2-yl)phenyl)pyridine-2,6-dicarboxamide)

There total 1 articles about 4,4'-(2,2'-dihydroxybiphenyl-3,3'-diyl)bis(N₂,N₆-bis(2-((S)-4-methyl-4,5-dihydrooxazol-2-yl)phenyl)pyridine-2,6-dicarboxamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

4,4'-(2,2'-bis(benzyloxy)biphenyl-3,3'-diyl)bis(N2,N6-bis(2-((S)-4-methyl-4,5-dihydrooxazol-2-yl)phenyl)pyridine-2,6-dicarboxamide) (1037078-41-3) → 4,4'-(2,2'-dihydroxybiphenyl-3,3'-diyl)bis(N2,N6-bis(2-((S)-4-methyl-4,5-dihydrooxazol-2-yl)phenyl)pyridine-2,6-dicarboxamide) (1037078-43-5)

Guidance literature:

With 10% Pd/C; hydrogen; In tetrahydrofuran; ethanol; for 48h; under 2585.81 Torr;

DOI:10.1021/ja802308a

Reference yield: 61.0%

4,4'-(2,2'-dihydroxybiphenyl-3,3'-diyl)bis(N2,N6-bis(2-((S)-4-methyl-4,5-dihydrooxazol-2-yl)phenyl)pyridine-2,6-dicarboxamide) (1037078-43-5) + chloro-diphenylphosphine (1079-66-9,74391-44-9) → 4,4'-(2,2'-bis(diphenylphosphinooxy)biphenyl-3,3'-diyl)bis(N2,N6-bis(2-((S)-4-methyl-4,5-dihydrooxazol-2-yl)phenyl)pyridine-2,6-dicarboxamide) (1112186-96-5)

Guidance literature:

With dmap; In tetrahydrofuran; for 4h; Inert atmosphere;

DOI:10.1021/ja802308a

upstream raw materials:

4,4'-(2,2'-bis(benzyloxy)biphenyl-3,3'-diyl)bis(N₂,N₆-bis(2-((S)-4-methyl-4,5-dihydrooxazol-2-yl)phenyl)pyridine-2,6-dicarboxamide)

Downstream raw materials:

4,4'-(2,2'-bis(diphenylphosphinooxy)biphenyl-3,3'-diyl)bis(N₂,N₆-bis(2-((S)-4-methyl-4,5-dihydrooxazol-2-yl)phenyl)pyridine-2,6-dicarboxamide)

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