4-(hexyloxy)-N-(4-(hexyloxy)phenyl)-N-(4-(thiophen-2-yl)phenyl)benzenamine

Base Information

Chemical Name:4-(hexyloxy)-N-(4-(hexyloxy)phenyl)-N-(4-(thiophen-2-yl)phenyl)benzenamine
CAS No.:1123693-92-4
Molecular Formula:C₃₄H₄₁NO₂S
Molecular Weight:527.771
Hs Code.:

Synonyms:4-(hexyloxy)-N-(4-(hexyloxy)phenyl)-N-(4-(thiophen-2-yl)phenyl)benzenamine

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Chemical Property of 4-(hexyloxy)-N-(4-(hexyloxy)phenyl)-N-(4-(thiophen-2-yl)phenyl)benzenamine

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Technology Process of 4-(hexyloxy)-N-(4-(hexyloxy)phenyl)-N-(4-(thiophen-2-yl)phenyl)benzenamine

There total 4 articles about 4-(hexyloxy)-N-(4-(hexyloxy)phenyl)-N-(4-(thiophen-2-yl)phenyl)benzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1092363-75-1
N,N-bis(4-hexyloxyphenyl)-4-bromophenylamine

: 54663-78-4
tributyl(thien-2-yl)stannane

: 1123693-92-4
4-(hexyloxy)-N-(4-(hexyloxy)phenyl)-N-(4-(thiophen-2-yl)phenyl)benzenamine

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; for 24h; Reflux; Inert atmosphere;
DOI:10.1016/j.tet.2012.12.071

Reference yield: 64.0%

: 6165-68-0
thiophene boronic acid

: 1092363-75-1
N,N-bis(4-hexyloxyphenyl)-4-bromophenylamine

: 1123693-92-4
4-(hexyloxy)-N-(4-(hexyloxy)phenyl)-N-(4-(thiophen-2-yl)phenyl)benzenamine

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate; In methanol; toluene; at 75 ℃; for 0.333333h; Microwave irradiation;
DOI:10.1002/anie.200804719

Reference yield:

: 1146433-75-1
4-(hexyloxy)-N-(4-(hexyloxy)phenyl)-N-phenylaniline

: 1123693-92-4
4-(hexyloxy)-N-(4-(hexyloxy)phenyl)-N-(4-(thiophen-2-yl)phenyl)benzenamine

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide / ethyl acetate / 24 h / 25 °C / Darkness

2: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; water / 16 h / Inert atmosphere; Reflux

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In tetrahydrofuran; water; ethyl acetate;
DOI:10.1021/ja311640f