C₁₁H₁₄O₅

Base Information

Chemical Name:C₁₁H₁₄O₅
CAS No.:1354784-87-4
Molecular Formula:C₁₁H₁₄O₅
Molecular Weight:226.229
Hs Code.:

C<sub>11</sub>H<sub>14</sub>O<sub>5</sub>

Synonyms:C₁₁H₁₄O₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₁H₁₄O₅

Chemical Property:

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Technology Process of C₁₁H₁₄O₅

There total 4 articles about C₁₁H₁₄O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1354784-99-8
C₁₄H₂₁NO₄

: 420-37-1
trimethoxonium tetrafluoroborate

: 1354784-87-4
C₁₁H₁₄O₅

Guidance literature:: C₁₄H₂₁NO₄; trimethoxonium tetrafluoroborate; With disodium hydrogenphosphate; In acetonitrile; at 20 ℃; for 3h;

With sodium hydrogencarbonate; In water; acetonitrile;
DOI:10.1016/j.tetlet.2011.11.062

Reference yield:

: 490-64-2
asaronic acid

: 1354784-87-4
C₁₁H₁₄O₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: pivaloyl chloride; triethylamine / tetrahydrofuran / 1 h / 0 °C

1.2: 5 h / 0 - 20 °C

2.1: N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium / tetrahydrofuran / 0.5 h / -78 °C

2.2: 2 h / -78 - -20 °C

3.1: boron trichloride / dichloromethane / 0.67 h / 20 °C

4.1: disodium hydrogenphosphate / acetonitrile / 3 h / 20 °C

With disodium hydrogenphosphate; N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; pivaloyl chloride; boron trichloride; triethylamine; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1016/j.tetlet.2011.11.062

Reference yield:

: 1354784-86-3
C₁₅H₂₃NO₄

: 1354784-87-4
C₁₁H₁₄O₅

Guidance literature:: Multi-step reaction with 2 steps

1: boron trichloride / dichloromethane / 0.67 h / 20 °C

2: disodium hydrogenphosphate / acetonitrile / 3 h / 20 °C

With disodium hydrogenphosphate; boron trichloride; In dichloromethane; acetonitrile;
DOI:10.1016/j.tetlet.2011.11.062