N-(4-bromo-2-nitrophenyl)-N-tert-butoxycarbonylcarbamic acid tert-butyl ester

Base Information

Chemical Name:N-(4-bromo-2-nitrophenyl)-N-tert-butoxycarbonylcarbamic acid tert-butyl ester
CAS No.:1228392-59-3
Molecular Formula:C₁₆H₂₁BrN₂O₆
Molecular Weight:417.257
Hs Code.:

Synonyms:N-(4-bromo-2-nitrophenyl)-N-tert-butoxycarbonylcarbamic acid tert-butyl ester

Suppliers and Price of N-(4-bromo-2-nitrophenyl)-N-tert-butoxycarbonylcarbamic acid tert-butyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 3 raw suppliers

Chemical Property of N-(4-bromo-2-nitrophenyl)-N-tert-butoxycarbonylcarbamic acid tert-butyl ester

Chemical Property:

Purity/Quality:: 98%+ ^*data from raw suppliers

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Technology Process of N-(4-bromo-2-nitrophenyl)-N-tert-butoxycarbonylcarbamic acid tert-butyl ester

There total 1 articles about N-(4-bromo-2-nitrophenyl)-N-tert-butoxycarbonylcarbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 875-51-4
4-Bromo-2-nitroaniline

: 1228392-59-3
N-(4-bromo-2-nitrophenyl)-N-tert-butoxycarbonylcarbamic acid tert-butyl ester

Guidance literature:: With dmap; In tetrahydrofuran; at 65 ℃;

Reference yield: 100.0%

: 5308-25-8
4-ethylpiperazine

: 1228392-59-3
N-(4-bromo-2-nitrophenyl)-N-tert-butoxycarbonylcarbamic acid tert-butyl ester

: tert-butyl (4-(4-ethylpiperazin-1-yl)-2-nitrophenyl)carbamate

Guidance literature:: With chloro(2-dicyclohexylphosphino-2′,6′-di-i-propoxy-1,1′-biphenyl)(2′-amino-1,1′-biphenyl-2-yl)-palladium(II); caesium carbonate; In toluene; at 95 - 105 ℃; Inert atmosphere;

Reference yield: 95.5%

: 4318-42-7
1-(1-methylethyl)piperazine

: 1228392-59-3
N-(4-bromo-2-nitrophenyl)-N-tert-butoxycarbonylcarbamic acid tert-butyl ester

: C₂₃H₃₆N₄O₆

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In toluene; at 80 ℃; for 3h; Inert atmosphere;