1-(trans-1-methyl-4-{[2-(methyloxy)ethyl]oxy}cyclohexyl)-4-piperidinone

Base Information

Chemical Name:1-(trans-1-methyl-4-{[2-(methyloxy)ethyl]oxy}cyclohexyl)-4-piperidinone
CAS No.:1134197-85-5
Molecular Formula:C₁₅H₂₇NO₃
Molecular Weight:269.384
Hs Code.:

Synonyms:1-(trans-1-methyl-4-{[2-(methyloxy)ethyl]oxy}cyclohexyl)-4-piperidinone

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Chemical Property of 1-(trans-1-methyl-4-{[2-(methyloxy)ethyl]oxy}cyclohexyl)-4-piperidinone

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Technology Process of 1-(trans-1-methyl-4-{[2-(methyloxy)ethyl]oxy}cyclohexyl)-4-piperidinone

There total 1 articles about 1-(trans-1-methyl-4-{[2-(methyloxy)ethyl]oxy}cyclohexyl)-4-piperidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.1%

: 1134197-84-4
trans-1-methyl-4-(2-methoxyethoxy)cyclohexylamine hydrochloride

: 77542-18-8
1-methyl-1-ethyl-4-oxopiperidinium iodide

: 1134197-85-5
1-(trans-1-methyl-4-{[2-(methyloxy)ethyl]oxy}cyclohexyl)-4-piperidinone

Guidance literature:: With potassium carbonate; In ethanol; water; at 80 ℃; for 2h;

Reference yield: 73.0%

: 1134197-85-5
1-(trans-1-methyl-4-{[2-(methyloxy)ethyl]oxy}cyclohexyl)-4-piperidinone

: 14543-43-2
3-amino-4-hydroxybenzonitrile

: 1134197-57-1
4-hydroxy-3-{[1-(trans-1-methyl-4-{[2-(methyloxy)ethyl]oxy}cyclohexyl)-4-piperidinyl]amino}benzonitrile

Guidance literature:: 1-(trans-1-methyl-4-{[2-(methyloxy)ethyl]oxy}cyclohexyl)-4-piperidinone; 3-amino-4-hydroxybenzonitrile; With polymer supported cyanoborohydride; acetic acid; In tetrahydrofuran; at 100 ℃; for 2h; Microwave;

With ammonia; In methanol; dichloromethane; Product distribution / selectivity;

Reference yield: 68.2%

: 1134197-85-5
1-(trans-1-methyl-4-{[2-(methyloxy)ethyl]oxy}cyclohexyl)-4-piperidinone

: 454-81-9
2-amino-4-(trifluoromethyl)phenol

: 1134198-18-7
2-{[1-(trans-1-methyl-4-{[2-(methyloxy)ethyl]oxy}cyclohexyl)-4-piperidinyl]amino}-4-(trifluoromethyl)phenol

Guidance literature:: 1-(trans-1-methyl-4-{[2-(methyloxy)ethyl]oxy}cyclohexyl)-4-piperidinone; 2-amino-4-(trifluoromethyl)phenol; With PS-CNBH₃; acetic acid; In dichloromethane; at 100 ℃; for 0.25h; Microwave;

With ammonia; In methanol; dichloromethane;