6-Bromo-2-fluoro-3-octyloxybenzonitrile

Base Information

Chemical Name:6-Bromo-2-fluoro-3-octyloxybenzonitrile
CAS No.:217816-62-1
Molecular Formula:C₁₅H₁₉BrFNO
Molecular Weight:328.224
Hs Code.:

Synonyms:6-Bromo-2-fluoro-3-octyloxybenzonitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-Bromo-2-fluoro-3-octyloxybenzonitrile

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Technology Process of 6-Bromo-2-fluoro-3-octyloxybenzonitrile

There total 4 articles about 6-Bromo-2-fluoro-3-octyloxybenzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 217816-56-3
6-Bromo-2-fluoro-3-octyloxybenzamide

: 217816-62-1
6-Bromo-2-fluoro-3-octyloxybenzonitrile

Guidance literature:: With thionyl chloride; In N,N-dimethyl-formamide; at 120 ℃; for 3h;
DOI:10.1039/a804525i

Reference yield:

: 119259-26-6
1-Bromo-3-fluoro-4-octyloxybenzene

: 217816-62-1
6-Bromo-2-fluoro-3-octyloxybenzonitrile

Guidance literature:: Multi-step reaction with 4 steps

1: 81 percent / LDA / tetrahydrofuran / 1.) -78 deg C, 1 h, 2.) -78 deg C to r.t.

2: oxalyl chloride, DMF / benzene / Ambient temperature

3: NH₄OH, H₂O / bis-(2-methoxy-ethyl) ether / Ambient temperature

4: 65 percent / SOCl₂ / dimethylformamide / 3 h / 120 °C

With ammonium hydroxide; thionyl chloride; oxalyl dichloride; water; N,N-dimethyl-formamide; lithium diisopropyl amide; In tetrahydrofuran; diethylene glycol dimethyl ether; N,N-dimethyl-formamide; benzene;
DOI:10.1039/a804525i

Reference yield:

: 217816-50-7
6-Bromo-2-fluoro-3-octyloxybenzoic acid

: 217816-62-1
6-Bromo-2-fluoro-3-octyloxybenzonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl chloride, DMF / benzene / Ambient temperature

2: NH₄OH, H₂O / bis-(2-methoxy-ethyl) ether / Ambient temperature

3: 65 percent / SOCl₂ / dimethylformamide / 3 h / 120 °C

With ammonium hydroxide; thionyl chloride; oxalyl dichloride; water; N,N-dimethyl-formamide; In diethylene glycol dimethyl ether; N,N-dimethyl-formamide; benzene;
DOI:10.1039/a804525i