9-(1-Methylethylidene)-1,4-diphenyl-5,6,7,8-tetrahydro-5,8-methanophthalazine

Base Information

Chemical Name:9-(1-Methylethylidene)-1,4-diphenyl-5,6,7,8-tetrahydro-5,8-methanophthalazine
CAS No.:362050-01-9
Molecular Formula:C₂₄H₂₂N₂
Molecular Weight:338.452
Hs Code.:

Synonyms:9-(1-Methylethylidene)-1,4-diphenyl-5,6,7,8-tetrahydro-5,8-methanophthalazine

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Chemical Property of 9-(1-Methylethylidene)-1,4-diphenyl-5,6,7,8-tetrahydro-5,8-methanophthalazine

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Technology Process of 9-(1-Methylethylidene)-1,4-diphenyl-5,6,7,8-tetrahydro-5,8-methanophthalazine

There total 4 articles about 9-(1-Methylethylidene)-1,4-diphenyl-5,6,7,8-tetrahydro-5,8-methanophthalazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 362050-13-3
2,3-dibenzoyl-7-(1-methylethylidene)bicyclo[2.2.1]hept-2-ene

: 362050-01-9
9-(1-Methylethylidene)-1,4-diphenyl-5,6,7,8-tetrahydro-5,8-methanophthalazine

Guidance literature:: With hydrazine hydrate; acetic acid; In ethanol; for 1h; Heating;
DOI:10.1039/b101330k

Reference yield:

: 2175-91-9
6,6'-dimethyl fulvene

: 362050-01-9
9-(1-Methylethylidene)-1,4-diphenyl-5,6,7,8-tetrahydro-5,8-methanophthalazine

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / benzene / 18 h / Heating

2: 93 percent / H₂ / 10percent Pd/C / ethyl acetate / 2.5 h / 20 °C

3: 85 percent / NH₂NH₂*H₂O; AcOH / aq. ethanol / 1 h / Heating

With hydrogen; hydrazine hydrate; acetic acid; 10percent Pd/C; In ethanol; ethyl acetate; benzene; 1: Diels-Alder reaction;
DOI:10.1039/b101330k

Reference yield:

: 1087-09-8
1,4-diphenyl-but-2-yne-1,4-dione

: 362050-01-9
9-(1-Methylethylidene)-1,4-diphenyl-5,6,7,8-tetrahydro-5,8-methanophthalazine

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / benzene / 18 h / Heating

2: 93 percent / H₂ / 10percent Pd/C / ethyl acetate / 2.5 h / 20 °C

3: 85 percent / NH₂NH₂*H₂O; AcOH / aq. ethanol / 1 h / Heating

With hydrogen; hydrazine hydrate; acetic acid; 10percent Pd/C; In ethanol; ethyl acetate; benzene; 1: Diels-Alder reaction;
DOI:10.1039/b101330k