(S)-tert-butyl N-(2-(4-((3-(2-hydroxy-1-(4-hydroxyphenyl)ethyl)thioureido)methyl)benzamido)phenyl)carbamate

Base Information

Chemical Name:(S)-tert-butyl N-(2-(4-((3-(2-hydroxy-1-(4-hydroxyphenyl)ethyl)thioureido)methyl)benzamido)phenyl)carbamate
CAS No.:1448350-43-3
Molecular Formula:C₂₈H₃₂N₄O₅S
Molecular Weight:536.652
Hs Code.:

Synonyms:(S)-tert-butyl N-(2-(4-((3-(2-hydroxy-1-(4-hydroxyphenyl)ethyl)thioureido)methyl)benzamido)phenyl)carbamate

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Chemical Property of (S)-tert-butyl N-(2-(4-((3-(2-hydroxy-1-(4-hydroxyphenyl)ethyl)thioureido)methyl)benzamido)phenyl)carbamate

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Technology Process of (S)-tert-butyl N-(2-(4-((3-(2-hydroxy-1-(4-hydroxyphenyl)ethyl)thioureido)methyl)benzamido)phenyl)carbamate

There total 6 articles about (S)-tert-butyl N-(2-(4-((3-(2-hydroxy-1-(4-hydroxyphenyl)ethyl)thioureido)methyl)benzamido)phenyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₀H₇ClF₃NO₂

: 1448350-43-3
(S)-tert-butyl N-(2-(4-((3-(2-hydroxy-1-(4-hydroxyphenyl)ethyl)thioureido)methyl)benzamido)phenyl)carbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: 20 h / 20 °C

2.1: potassium carbonate; methanol / water / 4 h / 70 °C

3.1: triethylamine / dichloromethane / 0.18 h / 20 °C

3.2: 0.17 h / 0 °C

4.1: acetonitrile / 17.5 h / 20 °C

With methanol; potassium carbonate; triethylamine; In dichloromethane; water; acetonitrile;
DOI:10.1021/jm400634n

Reference yield:

: 32462-30-9
(S)-hydroxyphenylglycine

: 1448350-43-3
(S)-tert-butyl N-(2-(4-((3-(2-hydroxy-1-(4-hydroxyphenyl)ethyl)thioureido)methyl)benzamido)phenyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate; iodine / tetrahydrofuran / 14 h / Reflux

2: acetonitrile / 17.5 h / 20 °C

With sodium tetrahydroborate; iodine; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jm400634n

Reference yield:

: 130029-61-7
4-[[(2,2,2-trifluoroacetyl)amino]methyl]benzoic acid

: 1448350-43-3
(S)-tert-butyl N-(2-(4-((3-(2-hydroxy-1-(4-hydroxyphenyl)ethyl)thioureido)methyl)benzamido)phenyl)carbamate

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine; oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide

2.1: 20 h / 20 °C

3.1: potassium carbonate; methanol / water / 4 h / 70 °C

4.1: triethylamine / dichloromethane / 0.18 h / 20 °C

4.2: 0.17 h / 0 °C

5.1: acetonitrile / 17.5 h / 20 °C

With methanol; oxalyl dichloride; potassium carbonate; triethylamine; In dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm400634n