4-(4-cyclohept-1-en-1-ylphenyl)-N-hydroxy-2-methyl-2-(methylsulfonyl)butanamide

Base Information

Chemical Name:4-(4-cyclohept-1-en-1-ylphenyl)-N-hydroxy-2-methyl-2-(methylsulfonyl)butanamide
CAS No.:1289620-59-2
Molecular Formula:C₁₉H₂₇NO₄S
Molecular Weight:365.494
Hs Code.:

Synonyms:4-(4-cyclohept-1-en-1-ylphenyl)-N-hydroxy-2-methyl-2-(methylsulfonyl)butanamide

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Chemical Property of 4-(4-cyclohept-1-en-1-ylphenyl)-N-hydroxy-2-methyl-2-(methylsulfonyl)butanamide

Chemical Property:

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Technology Process of 4-(4-cyclohept-1-en-1-ylphenyl)-N-hydroxy-2-methyl-2-(methylsulfonyl)butanamide

There total 3 articles about 4-(4-cyclohept-1-en-1-ylphenyl)-N-hydroxy-2-methyl-2-(methylsulfonyl)butanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1289627-20-8
C₂₄H₃₅NO₅S

: 1289620-59-2
4-(4-cyclohept-1-en-1-ylphenyl)-N-hydroxy-2-methyl-2-(methylsulfonyl)butanamide

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; dichloromethane; at 20 - 25 ℃; for 0.333333h;

Reference yield:

: 502-42-1
cycloheptanone

: 1289620-59-2
4-(4-cyclohept-1-en-1-ylphenyl)-N-hydroxy-2-methyl-2-(methylsulfonyl)butanamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 0.75 h / -78 °C

1.2: -78 - 25 °C

2.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 50 °C

3.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 0.33 h / 20 - 25 °C

With hydrogenchloride; sodium carbonate; lithium diisopropyl amide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; 2.1: Suzuki-Miyaura coupling;

Reference yield:

: 28075-51-6
cyclohept-1-en-1-yl trifluoromethanesulfonate

: 1289620-59-2
4-(4-cyclohept-1-en-1-ylphenyl)-N-hydroxy-2-methyl-2-(methylsulfonyl)butanamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 50 °C

2: hydrogenchloride / dichloromethane; 1,4-dioxane / 0.33 h / 20 - 25 °C

With hydrogenchloride; sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; dichloromethane; water; 1: Suzuki-Miyaura coupling;