ethyl 3-allyloxy-4-benzyloxybutyrate

Base Information

Chemical Name:ethyl 3-allyloxy-4-benzyloxybutyrate
CAS No.:693273-91-5
Molecular Formula:C₁₆H₂₂O₄
Molecular Weight:278.348
Hs Code.:

Synonyms:ethyl 3-allyloxy-4-benzyloxybutyrate

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Chemical Property of ethyl 3-allyloxy-4-benzyloxybutyrate

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Technology Process of ethyl 3-allyloxy-4-benzyloxybutyrate

There total 3 articles about ethyl 3-allyloxy-4-benzyloxybutyrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 81366-59-8
ethyl 4-(benzyloxy)-3-hydroxybutanoate

: 106-95-6
allyl bromide

: 693273-91-5
ethyl 3-allyloxy-4-benzyloxybutyrate

Guidance literature:: With calcium sulfate; silver(l) oxide; In benzene; at 20 ℃; for 11h;
DOI:10.1021/ol049493t

Reference yield:

: 60656-87-3
benzyloxyacetoaldehyde

: 693273-91-5
ethyl 3-allyloxy-4-benzyloxybutyrate

Guidance literature:: Multi-step reaction with 3 steps

1.1: SnCl₂ / CH₂Cl₂ / 0.25 h / 20 °C

1.2: 83 percent / CH₂Cl₂ / -10 - 20 °C

2.1: 70 percent / NaBH₄ / ethanol / 0.33 h / -10 °C

3.1: 93 percent / Ag₂O; CaSO₄ / benzene / 11 h / 20 °C

With calcium sulfate; sodium tetrahydroborate; tin(ll) chloride; silver(l) oxide; In ethanol; dichloromethane; benzene;
DOI:10.1021/ol049493t

Reference yield:

: 67354-34-1
ethyl 4-benzyloxyacetoacetate

: 693273-91-5
ethyl 3-allyloxy-4-benzyloxybutyrate

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / NaBH₄ / ethanol / 0.33 h / -10 °C

2: 93 percent / Ag₂O; CaSO₄ / benzene / 11 h / 20 °C

With calcium sulfate; sodium tetrahydroborate; silver(l) oxide; In ethanol; benzene;
DOI:10.1021/ol049493t