triethyl((2-methyl-1-((2R,3S)-2-methyl-3-vinyloxiran-2-yl)-12-phenyldodecan-2-yl)peroxy)silane

Base Information

Chemical Name:triethyl((2-methyl-1-((2R,3S)-2-methyl-3-vinyloxiran-2-yl)-12-phenyldodecan-2-yl)peroxy)silane
CAS No.:1341216-71-4
Molecular Formula:C₃₀H₅₂O₃Si
Molecular Weight:488.827
Hs Code.:

Synonyms:triethyl((2-methyl-1-((2R,3S)-2-methyl-3-vinyloxiran-2-yl)-12-phenyldodecan-2-yl)peroxy)silane

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Chemical Property of triethyl((2-methyl-1-((2R,3S)-2-methyl-3-vinyloxiran-2-yl)-12-phenyldodecan-2-yl)peroxy)silane

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Technology Process of triethyl((2-methyl-1-((2R,3S)-2-methyl-3-vinyloxiran-2-yl)-12-phenyldodecan-2-yl)peroxy)silane

There total 12 articles about triethyl((2-methyl-1-((2R,3S)-2-methyl-3-vinyloxiran-2-yl)-12-phenyldodecan-2-yl)peroxy)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 617-86-7
triethylsilane

: 1341216-62-3
(2R,3S)-2-methyl-2-(2-methylene-12-phenyldodecyl)-3-vinyloxirane

: 1341216-71-4
triethyl((2-methyl-1-((2R,3S)-2-methyl-3-vinyloxiran-2-yl)-12-phenyldodecan-2-yl)peroxy)silane

Guidance literature:: With Co(II) bis(2,2,6,6-tetramethylheptane-3,5-dienoate); oxygen; In 1,2-dichloro-ethane; at 20 ℃; under 760.051 Torr;
DOI:10.1055/s-0030-1260959

Reference yield:

: 1341216-63-4
(R)-4-methyl-6-(10-phenyldecyl)-5,6-dihydro-2H-pyran-2-one

: 1341216-71-4
triethyl((2-methyl-1-((2R,3S)-2-methyl-3-vinyloxiran-2-yl)-12-phenyldodecan-2-yl)peroxy)silane

Guidance literature:: Multi-step reaction with 7 steps

1.1: dihydrogen peroxide; sodium hydroxide / methanol; water / 0 - 20 °C / Inert atmosphere

2.1: sodium hydroxide / methanol; water / 2 h / 20 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

2.3: pH 3 - 4 / Inert atmosphere

3.1: diethyl ether; ethyl acetate / 0.17 h / 20 °C / Inert atmosphere

4.1: titanium(IV) dichlorodiisopropylate / tetrahydrofuran / 0 - 15 °C / Inert atmosphere

5.1: diisobutylaluminium hydride / hexane; toluene / -90 - -78 °C / Inert atmosphere

6.1: n-butyllithium / tetrahydrofuran / -78 - 0 °C / Inert atmosphere

6.2: Inert atmosphere

7.1: Co(II) bis(2,2,6,6-tetramethylheptane-3,5-dienoate); oxygen / 1,2-dichloro-ethane / 20 °C / 760.05 Torr

With n-butyllithium; titanium(IV) dichlorodiisopropylate; Co(II) bis(2,2,6,6-tetramethylheptane-3,5-dienoate); dihydrogen peroxide; oxygen; diisobutylaluminium hydride; sodium hydroxide; In tetrahydrofuran; methanol; diethyl ether; hexane; water; ethyl acetate; 1,2-dichloro-ethane; toluene;
DOI:10.1055/s-0030-1260959

Reference yield:

: C₂₂H₃₂O₄

: 1341216-71-4
triethyl((2-methyl-1-((2R,3S)-2-methyl-3-vinyloxiran-2-yl)-12-phenyldodecan-2-yl)peroxy)silane

Guidance literature:: Multi-step reaction with 5 steps

1.1: diethyl ether; ethyl acetate / 0.17 h / 20 °C / Inert atmosphere

2.1: titanium(IV) dichlorodiisopropylate / tetrahydrofuran / 0 - 15 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / hexane; toluene / -90 - -78 °C / Inert atmosphere

4.1: n-butyllithium / tetrahydrofuran / -78 - 0 °C / Inert atmosphere

4.2: Inert atmosphere

5.1: Co(II) bis(2,2,6,6-tetramethylheptane-3,5-dienoate); oxygen / 1,2-dichloro-ethane / 20 °C / 760.05 Torr

With n-butyllithium; titanium(IV) dichlorodiisopropylate; Co(II) bis(2,2,6,6-tetramethylheptane-3,5-dienoate); oxygen; diisobutylaluminium hydride; In tetrahydrofuran; diethyl ether; hexane; ethyl acetate; 1,2-dichloro-ethane; toluene;
DOI:10.1055/s-0030-1260959