3,6-di-tert-butyl-9-(2-(tetrahydro-2H-pyran-2-yloxy)-5-(2,4,4-trimethyl-pentan-2-yl)phenyl)-9H-carbazole

Base Information

Chemical Name:3,6-di-tert-butyl-9-(2-(tetrahydro-2H-pyran-2-yloxy)-5-(2,4,4-trimethyl-pentan-2-yl)phenyl)-9H-carbazole
CAS No.:1346129-63-2
Molecular Formula:C₃₉H₅₃NO₂
Molecular Weight:567.855
Hs Code.:

Synonyms:3,6-di-tert-butyl-9-(2-(tetrahydro-2H-pyran-2-yloxy)-5-(2,4,4-trimethyl-pentan-2-yl)phenyl)-9H-carbazole

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Chemical Property of 3,6-di-tert-butyl-9-(2-(tetrahydro-2H-pyran-2-yloxy)-5-(2,4,4-trimethyl-pentan-2-yl)phenyl)-9H-carbazole

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Technology Process of 3,6-di-tert-butyl-9-(2-(tetrahydro-2H-pyran-2-yloxy)-5-(2,4,4-trimethyl-pentan-2-yl)phenyl)-9H-carbazole

There total 6 articles about 3,6-di-tert-butyl-9-(2-(tetrahydro-2H-pyran-2-yloxy)-5-(2,4,4-trimethyl-pentan-2-yl)phenyl)-9H-carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 37500-95-1
3,6-di(tert-butyl)-9H-carbazole

: 1346129-62-1
2-(2-iodo-4-(2,4,4-trimethylpentan-2-yl)phenoxy)tetrahydro-2H-pyran

: 1346129-63-2
3,6-di-tert-butyl-9-(2-(tetrahydro-2H-pyran-2-yloxy)-5-(2,4,4-trimethyl-pentan-2-yl)phenyl)-9H-carbazole

Guidance literature:: With potassium phosphate; copper(l) iodide; N,N-dimethylethylenediamine; In toluene; at 120 ℃; for 96h; Schlenk technique; Inert atmosphere;

Reference yield: 67.01%

: 37500-95-1
3,6-di(tert-butyl)-9H-carbazole

: 1346129-62-1
2-(2-iodo-4-(2,4,4-trimethylpentan-2-yl)phenoxy)tetrahydro-2H-pyran

: 110-70-3
N,N`-dimethylethylenediamine

: 1346129-63-2
3,6-di-tert-butyl-9-(2-(tetrahydro-2H-pyran-2-yloxy)-5-(2,4,4-trimethyl-pentan-2-yl)phenyl)-9H-carbazole

Guidance literature:: With potassium phosphate; In toluene;

Reference yield:

: 140-66-9
tert-octylphenol

: 1346129-63-2
3,6-di-tert-butyl-9-(2-(tetrahydro-2H-pyran-2-yloxy)-5-(2,4,4-trimethyl-pentan-2-yl)phenyl)-9H-carbazole

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hypochlorite; sodium iodide; sodium hydroxide / water; methanol / 2 h / 0 °C

2: toluene-4-sulfonic acid / dichloromethane / 0.17 h / 0 - 20 °C

3: potassium phosphate; copper(l) iodide; N,N`-dimethylethylenediamine / toluene / 48 h / Inert atmosphere; Reflux

With sodium hypochlorite; potassium phosphate; copper(l) iodide; toluene-4-sulfonic acid; sodium iodide; sodium hydroxide; N,N`-dimethylethylenediamine; In methanol; dichloromethane; water; toluene;