Technology Process of C56H57N13O13S6
There total 6 articles about C56H57N13O13S6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
water; sodium hydroxide;
In
methanol;
at 22 ℃;
for 72h;
DOI:10.1021/jm201685h
- Guidance literature:
-
Multi-step reaction with 3 steps
1: toluene / 12 h / 75 °C
2: caesium carbonate / N,N-dimethyl-formamide / 48 h / 22 °C
3: water; sodium hydroxide / methanol / 72 h / 22 °C
With
water; caesium carbonate; sodium hydroxide;
In
methanol; N,N-dimethyl-formamide; toluene;
1: Curtius rearrangement;
DOI:10.1021/jm201685h
- Guidance literature:
-
Multi-step reaction with 6 steps
1: water; sodium hydroxide / tetrahydrofuran / 1.5 h / 60 °C
2: triethylamine / acetone / 1 h / Sonication
3: sodium azide / acetone / 1.33 h / 60 °C
4: toluene / 12 h / 75 °C
5: caesium carbonate / N,N-dimethyl-formamide / 48 h / 22 °C
6: water; sodium hydroxide / methanol / 72 h / 22 °C
With
sodium azide; water; caesium carbonate; triethylamine; sodium hydroxide;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide; acetone; toluene;
4: Curtius rearrangement;
DOI:10.1021/jm201685h