[methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosonoate]-(2->6)-4-O-acetyl-2-azido-3-O-benzyl-2-deoxy-D-galactopyranosyl trichloroacetimidate

Base Information

Chemical Name:[methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosonoate]-(2->6)-4-O-acetyl-2-azido-3-O-benzyl-2-deoxy-D-galactopyranosyl trichloroacetimidate
CAS No.:1021159-74-9
Molecular Formula:C₃₇H₄₆Cl₃N₅O₁₈
Molecular Weight:955.154
Hs Code.:

[methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosonoate]-(2->6)-4-O-acetyl-2-azido-3-O-benzyl-2-deoxy-D-galactopyranosyl trichloroacetimidate

Synonyms:[methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosonoate]-(2->6)-4-O-acetyl-2-azido-3-O-benzyl-2-deoxy-D-galactopyranosyl trichloroacetimidate

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Chemical Property of [methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosonoate]-(2->6)-4-O-acetyl-2-azido-3-O-benzyl-2-deoxy-D-galactopyranosyl trichloroacetimidate

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Technology Process of [methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosonoate]-(2->6)-4-O-acetyl-2-azido-3-O-benzyl-2-deoxy-D-galactopyranosyl trichloroacetimidate

There total 1 articles about [methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosonoate]-(2->6)-4-O-acetyl-2-azido-3-O-benzyl-2-deoxy-D-galactopyranosyl trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: [methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosonoate]-(2->6)-4-O-acetyl-2-azido-3-O-benzyl-2-deoxy-D-galactopyranoside

: 545-06-2
trichloroacetonitrile

: 1021159-74-9
[methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosonoate]-(2->6)-4-O-acetyl-2-azido-3-O-benzyl-2-deoxy-D-galactopyranosyl trichloroacetimidate

Guidance literature:: With potassium carbonate; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1021/jo702609p

Reference yield: 69.0%

: 1021159-74-9
[methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosonoate]-(2->6)-4-O-acetyl-2-azido-3-O-benzyl-2-deoxy-D-galactopyranosyl trichloroacetimidate

: 59524-02-6
N-tert-butoxycarbonyl-L-serine benzyl ester

: 1021159-75-0
N-tert-butoxycarbonyl O-[methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosonoate]-(2->6)-[4-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-galactopyranosyl]-L-serine benzyl ester

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In tetrahydrofuran; for 3h; cooling;
DOI:10.1021/jo702609p

Reference yield:

: 1021159-74-9
[methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosonoate]-(2->6)-4-O-acetyl-2-azido-3-O-benzyl-2-deoxy-D-galactopyranosyl trichloroacetimidate

: 73724-48-8
N-(fluoren-9-ylmethoxycarbonyl)-L-threonine benzyl ester

: C₆₁H₆₉N₅O₂₂

Guidance literature:: With thiophene; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; Inert atmosphere; Molecular sieve;
DOI:10.1021/jo8026164