dimethyl-4,4′-(anthracene-9,10-diyl)-dibenzoate

Base Information

Chemical Name:dimethyl-4,4′-(anthracene-9,10-diyl)-dibenzoate
CAS No.:1156005-02-5
Molecular Formula:C₃₀H₂₂O₄
Molecular Weight:446.502
Hs Code.:

Synonyms:dimethyl-4,4′-(anthracene-9,10-diyl)-dibenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dimethyl-4,4′-(anthracene-9,10-diyl)-dibenzoate

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Technology Process of dimethyl-4,4′-(anthracene-9,10-diyl)-dibenzoate

There total 2 articles about dimethyl-4,4′-(anthracene-9,10-diyl)-dibenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.5%

: 523-27-3
9,10-Dibromoanthracene

: 99768-12-4
4-methoxycarbonylphenylboronic acid

: 1156005-02-5
dimethyl-4,4′-(anthracene-9,10-diyl)-dibenzoate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In methanol; water; toluene; at 100 ℃; for 48h; Inert atmosphere;
DOI:10.1039/c2dt31844j

Reference yield: 13.0%

: 523-27-3
9,10-Dibromoanthracene

: 99768-12-4
4-methoxycarbonylphenylboronic acid

: 1279603-78-9
methyl 4-(10-bromoanthracen-9-yl)benzoate

: 1156005-02-5
dimethyl-4,4′-(anthracene-9,10-diyl)-dibenzoate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; cesium fluoride; In tetrahydrofuran; water; toluene; at 140 ℃; for 10h;
DOI:10.1016/j.cclet.2019.09.009