(R,E)-3-[4-(tert-butyldimethylsilanyloxymethyl)-2-phenyl-4,5-dihydrooxazol-4-yl]prop-2-en-1-ol

Base Information

Chemical Name:(R,E)-3-[4-(tert-butyldimethylsilanyloxymethyl)-2-phenyl-4,5-dihydrooxazol-4-yl]prop-2-en-1-ol
CAS No.:1049744-45-7
Molecular Formula:C₁₉H₂₉NO₃Si
Molecular Weight:347.53
Hs Code.:

Synonyms:(R,E)-3-[4-(tert-butyldimethylsilanyloxymethyl)-2-phenyl-4,5-dihydrooxazol-4-yl]prop-2-en-1-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R,E)-3-[4-(tert-butyldimethylsilanyloxymethyl)-2-phenyl-4,5-dihydrooxazol-4-yl]prop-2-en-1-ol

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Technology Process of (R,E)-3-[4-(tert-butyldimethylsilanyloxymethyl)-2-phenyl-4,5-dihydrooxazol-4-yl]prop-2-en-1-ol

There total 1 articles about (R,E)-3-[4-(tert-butyldimethylsilanyloxymethyl)-2-phenyl-4,5-dihydrooxazol-4-yl]prop-2-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1049744-53-7
C₂₁H₃₁NO₄Si

: 1049744-45-7
(R,E)-3-[4-(tert-butyldimethylsilanyloxymethyl)-2-phenyl-4,5-dihydrooxazol-4-yl]prop-2-en-1-ol

Guidance literature:: With boron trifluoride diethyl etherate; diisobutylaluminium hydride; In hexane; dichloromethane; at -78 - 20 ℃; for 2h;
DOI:10.1248/cpb.56.738

Reference yield: 93.0%

: 1049744-45-7
(R,E)-3-[4-(tert-butyldimethylsilanyloxymethyl)-2-phenyl-4,5-dihydrooxazol-4-yl]prop-2-en-1-ol

: 1049744-46-8
{(2R,3R)-3-[(4R)-4-(tert-butyldimethylsilanyloxymethyl)-2-phenyl-4,5-dihydrooxazol-4-yl]oxiranyl}methanol

Guidance literature:: With titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2S,3S)-tartrate; In dichloromethane; at -20 ℃; for 5h;
DOI:10.1248/cpb.56.738