Technology Process of 3-Ethoxy-N-hydroxy-4-methoxybenzenecarboximidamide
There total 3 articles about 3-Ethoxy-N-hydroxy-4-methoxybenzenecarboximidamide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydroxylamine hydrochloride; sodium carbonate;
In
ethanol; water;
at 0 ℃;
for 18h;
Reflux;
DOI:10.1016/j.ejmech.2011.03.031
- Guidance literature:
-
Multi-step reaction with 3 steps
1: formic acid; hydroxylamine hydrochloride; sodium formate / 3 h / 125 °C
2: potassium carbonate / N,N-dimethyl-formamide
3: hydroxylamine hydrochloride; sodium hydroxide / ethanol; water / 18 h / 0 °C / Reflux
With
formic acid; hydroxylamine hydrochloride; sodium formate; potassium carbonate; sodium hydroxide;
In
ethanol; water; N,N-dimethyl-formamide;
DOI:10.1111/j.1747-0285.2011.01304.x
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate / N,N-dimethyl-formamide
2: hydroxylamine hydrochloride; sodium hydroxide / ethanol; water / 18 h / 0 °C / Reflux
With
hydroxylamine hydrochloride; potassium carbonate; sodium hydroxide;
In
ethanol; water; N,N-dimethyl-formamide;
DOI:10.1111/j.1747-0285.2011.01304.x