Technology Process of C18H29N3O4
There total 5 articles about C18H29N3O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
(6R)-4-(methoxymethyl)-6-methylmorpholin-3-one;
With
n-butyllithium; diisopropylamine;
In
tetrahydrofuran; hexane;
at -78 ℃;
for 1.5h;
1-(trans-4-methylcyclohexyl)-1H-imidazole-4-carbaldehyde;
In
tetrahydrofuran; hexane;
at -78 - 20 ℃;
for 14.5h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydride / tetrahydrofuran / 1.5 h / 20 °C / Cooling with ice
1.2: 20 °C / Cooling with ice
2.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 1.5 h / -78 °C
2.2: 14.5 h / -78 - 20 °C
With
n-butyllithium; sodium hydride; diisopropylamine;
In
tetrahydrofuran; hexane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 4 h / 70 °C
2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C
3.1: sodium hydrogencarbonate; iodine; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / water; toluene / 2 h / 20 °C
4.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 1.5 h / -78 °C
4.2: 14.5 h / -78 - 20 °C
With
lithium aluminium tetrahydride; n-butyllithium; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; iodine; sodium hydrogencarbonate; diisopropylamine;
In
tetrahydrofuran; hexane; water; toluene;