4-[3,6,10-Tris-(2-nitro-benzenesulfonyl)-3,6,10,16-tetraaza-bicyclo[10.3.1]hexadeca-1⁽¹⁵⁾,12⁽¹⁶⁾,13-trien-14-yl]-piperazine-1-carboxylic acid tert-butyl ester

Base Information

• Chemical Name: 4-[3,6,10-Tris-(2-nitro-benzenesulfonyl)-3,6,10,16-tetraaza-bicyclo[10.3.1]hexadeca-1⁽¹⁵⁾,12⁽¹⁶⁾,13-trien-14-yl]-piperazine-1-carboxylic acid tert-butyl ester
• CAS No.: 215164-34-4
• Molecular Formula: C₃₉H₄₅N₉O₁₄S₃
• Molecular Weight: 960.036

Synonyms:4-[3,6,10-Tris-(2-nitro-benzenesulfonyl)-3,6,10,16-tetraaza-bicyclo[10.3.1]hexadeca-1⁽¹⁵⁾,12⁽¹⁶⁾,13-trien-14-yl]-piperazine-1-carboxylic acid tert-butyl ester

Chemical Property of 4-[3,6,10-Tris-(2-nitro-benzenesulfonyl)-3,6,10,16-tetraaza-bicyclo[10.3.1]hexadeca-1⁽¹⁵⁾,12⁽¹⁶⁾,13-trien-14-yl]-piperazine-1-carboxylic acid tert-butyl ester

Chemical Property:

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Technology Process of 4-[3,6,10-Tris-(2-nitro-benzenesulfonyl)-3,6,10,16-tetraaza-bicyclo[10.3.1]hexadeca-1⁽¹⁵⁾,12⁽¹⁶⁾,13-trien-14-yl]-piperazine-1-carboxylic acid tert-butyl ester

There total 4 articles about 4-[3,6,10-Tris-(2-nitro-benzenesulfonyl)-3,6,10,16-tetraaza-bicyclo[10.3.1]hexadeca-1⁽¹⁵⁾,12⁽¹⁶⁾,13-trien-14-yl]-piperazine-1-carboxylic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) → 4-[3,6,10-Tris-(2-nitro-benzenesulfonyl)-3,6,10,16-tetraaza-bicyclo[10.3.1]hexadeca-1(15),12(16),13-trien-14-yl]-piperazine-1-carboxylic acid tert-butyl ester (215164-34-4)

Guidance literature:

Multi-step reaction with 3 steps

1: Et₃N

2: aq. NaOH / tetrahydrofuran

3: Cs₂CO₃ / dimethylformamide

With sodium hydroxide; caesium carbonate; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1016/S0960-894X(98)00424-7

Reference yield:

4-piperazinyl-2,6-bis-hydroxymethyl pyridine (215164-31-1) → 4-[3,6,10-Tris-(2-nitro-benzenesulfonyl)-3,6,10,16-tetraaza-bicyclo[10.3.1]hexadeca-1(15),12(16),13-trien-14-yl]-piperazine-1-carboxylic acid tert-butyl ester (215164-34-4)

Guidance literature:

Multi-step reaction with 3 steps

1: Et₃N

2: aq. NaOH / tetrahydrofuran

3: Cs₂CO₃ / dimethylformamide

With sodium hydroxide; caesium carbonate; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1016/S0960-894X(98)00424-7

Reference yield:

4-[N4'-(t-Boc)-piperazin-N1'-yl]pyridine-2,6-dimethanol (215164-32-2) → 4-[3,6,10-Tris-(2-nitro-benzenesulfonyl)-3,6,10,16-tetraaza-bicyclo[10.3.1]hexadeca-1(15),12(16),13-trien-14-yl]-piperazine-1-carboxylic acid tert-butyl ester (215164-34-4)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. NaOH / tetrahydrofuran

2: Cs₂CO₃ / dimethylformamide

With sodium hydroxide; caesium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1016/S0960-894X(98)00424-7

upstream raw materials:

4-[2,6-Bis-(toluene-4-sulfonyloxymethyl)-pyridin-4-yl]-piperazine-1-carboxylic acid tert-butyl ester

N¹,N³,N⁶-tris(2-nitrobenzenesulfonyl)-1,6-diamino-3-azahexane

di-tert-butyl dicarbonate

4-piperazinyl-2,6-bis-hydroxymethyl pyridine

Downstream raw materials:

14-piperazinyl-3,6,10-tris(2-nitrobenzenesulfonyl)-3,6,10,16-tetraazabicyclo[10.3.1]hexadeca-1⁽¹⁶⁾,12,14-triene

14-[N⁴-(1-pyrenebutyryl)piperazin-N¹-yl]-3,6,10-tris(2-nitrobenzenesulfonyl)-3,6,10,16-tetraazabicyclo[10.3.1]hexadeca-1⁽¹⁶⁾,12,14-triene

14-[N⁴-(2-anthraquinonemethyl)piperazin-N¹-yl]-3,6,10-tris(2-nitrobenzenesulfonyl)-3,6,10,16-tetraazabicyclo[10.3.1]hexadeca-1⁽¹⁶⁾,12,14-triene

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