N-2-hydroxyethyl-N-oleyl-N-n-octadecylamine O-tert-butyldiphenylsilyl ether

Base Information

Chemical Name:N-2-hydroxyethyl-N-oleyl-N-n-octadecylamine O-tert-butyldiphenylsilyl ether
CAS No.:252579-89-8
Molecular Formula:C₅₄H₉₅NOSi
Molecular Weight:802.44
Hs Code.:

Synonyms:N-2-hydroxyethyl-N-oleyl-N-n-octadecylamine O-tert-butyldiphenylsilyl ether

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-2-hydroxyethyl-N-oleyl-N-n-octadecylamine O-tert-butyldiphenylsilyl ether

Chemical Property:

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Technology Process of N-2-hydroxyethyl-N-oleyl-N-n-octadecylamine O-tert-butyldiphenylsilyl ether

There total 4 articles about N-2-hydroxyethyl-N-oleyl-N-n-octadecylamine O-tert-butyldiphenylsilyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 139897-19-1
(2-bromoethoxy)(tert-butyl)diphenylsilane

: 173790-60-8
N-octadecyloctadec-9-en-1-amine

: 252579-89-8
N-2-hydroxyethyl-N-oleyl-N-n-octadecylamine O-tert-butyldiphenylsilyl ether

Guidance literature:: With potassium carbonate; In ethyl acetate; for 48h; Heating;
DOI:10.1021/jm9806446

Reference yield:

: 2423-10-1
Oleic aldehyde

: 252579-89-8
N-2-hydroxyethyl-N-oleyl-N-n-octadecylamine O-tert-butyldiphenylsilyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: anhyd MgSO₄ / CH₂Cl₂ / 3 h / 0 - 20 °C

2: NaBH₄ / CH₂Cl₂; methanol / 4 h / 0 - 20 °C

3: 47 percent / K₂CO₃ / ethyl acetate / 48 h / Heating

With sodium tetrahydroborate; magnesium sulfate; potassium carbonate; In methanol; dichloromethane; ethyl acetate; 1: Condensation / 2: Reduction / 3: Substitution;
DOI:10.1021/jm9806446

Reference yield:

: 124-30-1
1-aminooctadecane

: 252579-89-8
N-2-hydroxyethyl-N-oleyl-N-n-octadecylamine O-tert-butyldiphenylsilyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: anhyd MgSO₄ / CH₂Cl₂ / 3 h / 0 - 20 °C

2: NaBH₄ / CH₂Cl₂; methanol / 4 h / 0 - 20 °C

3: 47 percent / K₂CO₃ / ethyl acetate / 48 h / Heating

With sodium tetrahydroborate; magnesium sulfate; potassium carbonate; In methanol; dichloromethane; ethyl acetate; 1: Condensation / 2: Reduction / 3: Substitution;
DOI:10.1021/jm9806446