(2S,3S,8S,9S,4E,6E)-3-tert-butoxycarbonylamino-9-methoxy-2,6,8-trimethyl-1-p-methoxybenzyloxy-4,6-decadiene

Base Information

Chemical Name:(2S,3S,8S,9S,4E,6E)-3-tert-butoxycarbonylamino-9-methoxy-2,6,8-trimethyl-1-p-methoxybenzyloxy-4,6-decadiene
CAS No.:238745-93-2
Molecular Formula:C₃₃H₄₇NO₅
Molecular Weight:537.74
Hs Code.:

Synonyms:(2S,3S,8S,9S,4E,6E)-3-tert-butoxycarbonylamino-9-methoxy-2,6,8-trimethyl-1-p-methoxybenzyloxy-4,6-decadiene

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Chemical Property of (2S,3S,8S,9S,4E,6E)-3-tert-butoxycarbonylamino-9-methoxy-2,6,8-trimethyl-1-p-methoxybenzyloxy-4,6-decadiene

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Technology Process of (2S,3S,8S,9S,4E,6E)-3-tert-butoxycarbonylamino-9-methoxy-2,6,8-trimethyl-1-p-methoxybenzyloxy-4,6-decadiene

There total 8 articles about (2S,3S,8S,9S,4E,6E)-3-tert-butoxycarbonylamino-9-methoxy-2,6,8-trimethyl-1-p-methoxybenzyloxy-4,6-decadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 238746-03-7
(2R,3S)-2-azido-4-(p-methoxybenzyloxy)-3-methyl-1-butanol

: 238745-93-2
(2S,3S,8S,9S,4E,6E)-3-tert-butoxycarbonylamino-9-methoxy-2,6,8-trimethyl-1-p-methoxybenzyloxy-4,6-decadiene

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / H₂ / 10 percent Pd/C / methanol / 0.67 h

2: CH₂Cl₂

3: 94 percent / Dess-Martin reagent / CH₂Cl₂ / 1 h

4: 1.) LDA / 1.) THF, 10 min, 2.) THF, 10 min

With hydrogen; Dess-Martin periodane; lithium diisopropyl amide; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1021/ja9811243

Reference yield:

: (1R,2R,6S,8R)-4-[(2S,3S)-2-Azido-4-(4-methoxy-benzyloxy)-3-methyl-butyl]-2,9,9-trimethyl-3,5-dioxa-4-bora-tricyclo[6.1.1.0^2,6]decane

: 238745-93-2
(2S,3S,8S,9S,4E,6E)-3-tert-butoxycarbonylamino-9-methoxy-2,6,8-trimethyl-1-p-methoxybenzyloxy-4,6-decadiene

Guidance literature:: Multi-step reaction with 5 steps

1: 75 percent / H₂O₂, aq. NaOH

2: 100 percent / H₂ / 10 percent Pd/C / methanol / 0.67 h

3: CH₂Cl₂

4: 94 percent / Dess-Martin reagent / CH₂Cl₂ / 1 h

5: 1.) LDA / 1.) THF, 10 min, 2.) THF, 10 min

With sodium hydroxide; hydrogen; dihydrogen peroxide; Dess-Martin periodane; lithium diisopropyl amide; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1021/ja9811243

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 238745-93-2
(2S,3S,8S,9S,4E,6E)-3-tert-butoxycarbonylamino-9-methoxy-2,6,8-trimethyl-1-p-methoxybenzyloxy-4,6-decadiene

Guidance literature:: Multi-step reaction with 3 steps

1: CH₂Cl₂

2: 94 percent / Dess-Martin reagent / CH₂Cl₂ / 1 h

3: 1.) LDA / 1.) THF, 10 min, 2.) THF, 10 min

With Dess-Martin periodane; lithium diisopropyl amide; In dichloromethane;
DOI:10.1021/ja9811243