benzyl N-(benzyloxycarbonyl)-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-L-serinate

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Chemical Name:benzyl N-(benzyloxycarbonyl)-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-L-serinate
CAS No.:1332305-10-8
Molecular Formula:C₅₂H₄₅NO₁₄
Molecular Weight:907.928
Hs Code.:

Synonyms:benzyl N-(benzyloxycarbonyl)-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-L-serinate

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Chemical Property of benzyl N-(benzyloxycarbonyl)-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-L-serinate

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Technology Process of benzyl N-(benzyloxycarbonyl)-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-L-serinate

There total 9 articles about benzyl N-(benzyloxycarbonyl)-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-L-serinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 21209-51-8
N-benzyloxycarbonyl-L-serine benzyl ester

: 2,3,4,6-tetra-O-benzoyl-D-glucopyranosyl o-isopropenylphenylacetate

: 1332305-10-8
benzyl N-(benzyloxycarbonyl)-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-L-serinate

Guidance literature:: N-benzyloxycarbonyl-L-serine benzyl ester; 2,3,4,6-tetra-O-benzoyl-D-glucopyranosyl o-isopropenylphenylacetate; In dichloromethane; at 0 ℃; for 0.5h; Molecular sieve;

With bis(trifluoromethanesulfonyl)amide; In dichloromethane; at 0 - 20 ℃; Molecular sieve;
DOI:10.1002/ejoc.202101367

Reference yield: 86.0%

: 21209-51-8
N-benzyloxycarbonyl-L-serine benzyl ester

: 172847-85-7
(2R,3R,4S,5R,6S)-2-((benzoyloxy)methyl)-6-(p-tolylthio)tetrahydro-2H-pyran-3,4,5-triyl tribenzoate

: 1332305-10-8
benzyl N-(benzyloxycarbonyl)-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-L-serinate

Guidance literature:: With copper(II) bis(trifluoromethanesulfonate); In dichloromethane; at 20 ℃; for 22h; Molecular sieve; Inert atmosphere; UV-irradiation;
DOI:10.1021/acs.orglett.5b02823

Reference yield: 84.0%

: 1221151-98-9
2,3,4,6-tetra-O-benzoyl-D-glucopyranosyl ortho-(hex-1-ynyl)benzoate

: 21209-51-8
N-benzyloxycarbonyl-L-serine benzyl ester

: 1332305-10-8
benzyl N-(benzyloxycarbonyl)-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-L-serinate

Guidance literature:: 2,3,4,6-tetra-O-benzoyl-D-glucopyranosyl ortho-(hex-1-ynyl)benzoate; N-benzyloxycarbonyl-L-serine benzyl ester; In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere; Molecular sieve;

With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere; Molecular sieve;
DOI:10.1021/acs.joc.1c00151