2-phenylamino-(3,4,6-tri-O-acetyl-1,2-dideoxy-α-D-glucopyrano)<2,1-d>-2-thiazoline

Base Information

Chemical Name:2-phenylamino-(3,4,6-tri-O-acetyl-1,2-dideoxy-α-D-glucopyrano)<2,1-d>-2-thiazoline
CAS No.:158315-63-0
Molecular Formula:C₁₉H₂₂N₂O₇S
Molecular Weight:422.459
Hs Code.:

Synonyms:2-phenylamino-(3,4,6-tri-O-acetyl-1,2-dideoxy-α-D-glucopyrano)<2,1-d>-2-thiazoline

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Chemical Property of 2-phenylamino-(3,4,6-tri-O-acetyl-1,2-dideoxy-α-D-glucopyrano)<2,1-d>-2-thiazoline

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Technology Process of 2-phenylamino-(3,4,6-tri-O-acetyl-1,2-dideoxy-α-D-glucopyrano)<2,1-d>-2-thiazoline

There total 3 articles about 2-phenylamino-(3,4,6-tri-O-acetyl-1,2-dideoxy-α-D-glucopyrano)<2,1-d>-2-thiazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 158315-51-6
1,3,4,6-tetra-O-acetyl-2-deoxy-2-(3-phenylthioureido)-α-D-glucopyranose

: 158315-63-0
2-phenylamino-(3,4,6-tri-O-acetyl-1,2-dideoxy-α-D-glucopyrano)<2,1-d>-2-thiazoline

Guidance literature:: With tin(IV) chloride; In dichloromethane; for 24h; Ambient temperature;
DOI:10.1016/S0040-4020(01)81122-4

Reference yield:

: 10034-19-2,1191127-63-5
1,3,4,6-tetra-O-acetyl-2-amino-2-deoxy-α-D-glucopyranose hydrochloride

: 158315-63-0
2-phenylamino-(3,4,6-tri-O-acetyl-1,2-dideoxy-α-D-glucopyrano)<2,1-d>-2-thiazoline

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) CaCO₃ / 1.) water, CH₂Cl₂, RT, 30 min; 2.) RT, 24 h

2: 89 percent / SnCl₄ / CH₂Cl₂ / 24 h / Ambient temperature

With tin(IV) chloride; calcium carbonate; In dichloromethane;
DOI:10.1016/S0040-4020(01)81122-4

Reference yield:

: 103-72-0
phenyl isothiocyanate

: 158315-63-0
2-phenylamino-(3,4,6-tri-O-acetyl-1,2-dideoxy-α-D-glucopyrano)<2,1-d>-2-thiazoline

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) CaCO₃ / 1.) water, CH₂Cl₂, RT, 30 min; 2.) RT, 24 h

2: 89 percent / SnCl₄ / CH₂Cl₂ / 24 h / Ambient temperature

With tin(IV) chloride; calcium carbonate; In dichloromethane;
DOI:10.1016/S0040-4020(01)81122-4