(4-[1-(4-trifluoromethoxyphenyl)-1H-[1,2,4]triazol-3-yl]phenyl)carbamic acid 1,1-dimethylprop-2-ynyl ester

Base Information

Chemical Name:(4-[1-(4-trifluoromethoxyphenyl)-1H-[1,2,4]triazol-3-yl]phenyl)carbamic acid 1,1-dimethylprop-2-ynyl ester
CAS No.:1265173-52-1
Molecular Formula:C₂₁H₁₇F₃N₄O₃
Molecular Weight:430.386
Hs Code.:

Synonyms:(4-[1-(4-trifluoromethoxyphenyl)-1H-[1,2,4]triazol-3-yl]phenyl)carbamic acid 1,1-dimethylprop-2-ynyl ester

Suppliers and Price of (4-[1-(4-trifluoromethoxyphenyl)-1H-[1,2,4]triazol-3-yl]phenyl)carbamic acid 1,1-dimethylprop-2-ynyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (4-[1-(4-trifluoromethoxyphenyl)-1H-[1,2,4]triazol-3-yl]phenyl)carbamic acid 1,1-dimethylprop-2-ynyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (4-[1-(4-trifluoromethoxyphenyl)-1H-[1,2,4]triazol-3-yl]phenyl)carbamic acid 1,1-dimethylprop-2-ynyl ester

There total 4 articles about (4-[1-(4-trifluoromethoxyphenyl)-1H-[1,2,4]triazol-3-yl]phenyl)carbamic acid 1,1-dimethylprop-2-ynyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 32315-10-9
bis(trichloromethyl) carbonate

: 1181214-75-4
4-(1-(4-(trifluoromethoxy)phenyl)-1H-1,2,4-triazol-3-yl)aniline

: 115-19-5
2-methyl-but-3-yn-2-ol

: 1265173-52-1
(4-[1-(4-trifluoromethoxyphenyl)-1H-[1,2,4]triazol-3-yl]phenyl)carbamic acid 1,1-dimethylprop-2-ynyl ester

Guidance literature:: bis(trichloromethyl) carbonate; 2-methyl-but-3-yn-2-ol; With pyridine; In dichloromethane; at 23 ℃; for 1h;

4-(1-(4-(trifluoromethoxy)phenyl)-1H-1,2,4-triazol-3-yl)aniline; In dichloromethane; at 23 ℃; for 3h;

Reference yield:

: 1181214-76-5
3-(4-nitrophenyl)-1-(4-(trifluoromethoxy)phenyl)-1H-1,2,4-triazole

: 1265173-52-1
(4-[1-(4-trifluoromethoxyphenyl)-1H-[1,2,4]triazol-3-yl]phenyl)carbamic acid 1,1-dimethylprop-2-ynyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogen / palladium on activated charcoal / ethanol

2.1: pyridine / dichloromethane / 1 h / 23 °C

2.2: 3 h / 23 °C

With pyridine; hydrogen; palladium on activated charcoal; In ethanol; dichloromethane;

Reference yield:

: 1181214-77-6
1-(4-nitrobenzylidene)-2-(4-(trifluoromethoxy)phenyl)hydrazine

: 1265173-52-1
(4-[1-(4-trifluoromethoxyphenyl)-1H-[1,2,4]triazol-3-yl]phenyl)carbamic acid 1,1-dimethylprop-2-ynyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-Bromosuccinimide; dimethylsulfide / dichloromethane / 2 h / -20 - 20 °C / Inert atmosphere

2.1: triethylamine / ethanol / 2 h / Reflux

3.1: hydrogen / palladium on activated charcoal / ethanol

4.1: pyridine / dichloromethane / 1 h / 23 °C

4.2: 3 h / 23 °C

With pyridine; N-Bromosuccinimide; dimethylsulfide; hydrogen; triethylamine; palladium on activated charcoal; In ethanol; dichloromethane;