dibutyl-(2-O-benzoyl-3,4-di-O-benzyl-6-O-triisopropylsilyl-α-D-mannopyranosyl) phosphate

Base Information

Chemical Name:dibutyl-(2-O-benzoyl-3,4-di-O-benzyl-6-O-triisopropylsilyl-α-D-mannopyranosyl) phosphate
CAS No.:1092958-76-3
Molecular Formula:C₄₄H₆₅O₁₀PSi
Molecular Weight:813.053
Hs Code.:

Synonyms:dibutyl-(2-O-benzoyl-3,4-di-O-benzyl-6-O-triisopropylsilyl-α-D-mannopyranosyl) phosphate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dibutyl-(2-O-benzoyl-3,4-di-O-benzyl-6-O-triisopropylsilyl-α-D-mannopyranosyl) phosphate

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Technology Process of dibutyl-(2-O-benzoyl-3,4-di-O-benzyl-6-O-triisopropylsilyl-α-D-mannopyranosyl) phosphate

There total 1 articles about dibutyl-(2-O-benzoyl-3,4-di-O-benzyl-6-O-triisopropylsilyl-α-D-mannopyranosyl) phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 13154-24-0
triisopropylsilyl chloride

: 1059116-10-7
dibutyl (2-O-benzoyl-3,4-di-O-benzyl-α-D-mannopyranosyl) phosphate

: 1092958-76-3
dibutyl-(2-O-benzoyl-3,4-di-O-benzyl-6-O-triisopropylsilyl-α-D-mannopyranosyl) phosphate

Guidance literature:: With pyridine; dmap; In dichloromethane; at 20 ℃; for 36h; Inert atmosphere;
DOI:10.1021/ja806283e

Reference yield: 100.0%

: C₄₁H₄₂O₆

: 1092958-76-3
dibutyl-(2-O-benzoyl-3,4-di-O-benzyl-6-O-triisopropylsilyl-α-D-mannopyranosyl) phosphate

: (2-O-benzoyl-3,4-di-O-benzyl-6-O-triisopropylsilyl-α-D-mannopyranosyl)-(1->6)-1-O-allyl-2-O-napthylmethyl-3,4,5-tri-O-benzyl-D-myo-inositol

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In toluene; at -40 - 20 ℃; Inert atmosphere;
DOI:10.1021/ja806283e

Reference yield: 75.0%

: 1092958-76-3
dibutyl-(2-O-benzoyl-3,4-di-O-benzyl-6-O-triisopropylsilyl-α-D-mannopyranosyl) phosphate

: 346441-51-8
1-O-allyl-2-O-benzoyl-3,4-di-O-benzyl-α-D-mannopyranose

: 346441-53-0
allyl O-(2-O-benzoyl-3,4-di-O-benzyl-α-D-mannopyranosyl)-(1→6)-2-O-benzoyl-3,4-di-O-benzyl-α-D-mannopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 1.5h; Inert atmosphere;
DOI:10.1021/acs.joc.8b02944