Technology Process of C23H30O4
There total 10 articles about C23H30O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: sodium iodide / acetone / 24 h / Reflux
2: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C
3: ozone / dichloromethane / 0.25 h / -78 °C
4: diethyl ether / diethyl ether; dichloromethane / 0.75 h / -78 °C
5: methanol; toluene-4-sulfonic acid / 6 h / Reflux
6: pyridinium p-toluenesulfonate / 3 h / 20 °C
7: methanol; potassium carbonate / 2 h / 20 °C
With
methanol; diethyl ether; potassium tert-butylate; pyridinium p-toluenesulfonate; potassium carbonate; toluene-4-sulfonic acid; ozone; sodium iodide;
In
tetrahydrofuran; diethyl ether; dichloromethane; acetone;
DOI:10.1016/j.tetlet.2011.09.134
- Guidance literature:
-
Multi-step reaction with 6 steps
1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C
2: ozone / dichloromethane / 0.25 h / -78 °C
3: diethyl ether / diethyl ether; dichloromethane / 0.75 h / -78 °C
4: methanol; toluene-4-sulfonic acid / 6 h / Reflux
5: pyridinium p-toluenesulfonate / 3 h / 20 °C
6: methanol; potassium carbonate / 2 h / 20 °C
With
methanol; diethyl ether; potassium tert-butylate; pyridinium p-toluenesulfonate; potassium carbonate; toluene-4-sulfonic acid; ozone;
In
tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1016/j.tetlet.2011.09.134