Technology Process of 4,4,5,5-tetramethyl-2-(4-(pentacen-6-yl)phenyl)imidazolidine-1,3-dioxyl
There total 3 articles about 4,4,5,5-tetramethyl-2-(4-(pentacen-6-yl)phenyl)imidazolidine-1,3-dioxyl which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium periodate;
In
dichloromethane; water;
for 0.5h;
Darkness;
DOI:10.1002/anie.201300595
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: magnesium / tetrahydrofuran / 1 h / Inert atmosphere; Heating
1.2: 2 h / Inert atmosphere
1.3: 0.08 h / Darkness
2.1: potassium carbonate / dichloromethane; methanol / 72 h / Reflux; Inert atmosphere; Darkness
3.1: sodium periodate / dichloromethane; water / 0.5 h / Darkness
With
sodium periodate; potassium carbonate; magnesium;
In
tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1002/anie.201300595
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sulfuric acid / water / 20 °C
1.2: 1 h / 90 °C / Inert atmosphere
2.1: magnesium / tetrahydrofuran / 1 h / 50 °C / Inert atmosphere
2.2: 2 h / 59 °C / Inert atmosphere
2.3: 0.08 h / 20 °C / Darkness
3.1: potassium carbonate / dichloromethane; methanol / 72 h / Inert atmosphere; Darkness; Reflux
4.1: sodium periodate / water; dichloromethane / 0.5 h / Darkness
With
sodium periodate; sulfuric acid; potassium carbonate; magnesium;
In
tetrahydrofuran; methanol; dichloromethane; water;
