Technology Process of C15H22N2O4
There total 4 articles about C15H22N2O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
1,8-diazabicyclo[5.4.0]undec-7-ene;
In
acetonitrile;
DOI:10.1021/ja073340u
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydroxide / tetrahydrofuran
2: sodium hydrogencarbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide; dichloromethane / 0 - 20 °C / Inert atmosphere
3: dichloromethane; diethyl ether / Inert atmosphere
4: mercaptoacetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / Inert atmosphere
With
sodium hydrogencarbonate; benzotriazol-1-ol; mercaptoacetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide;
In
tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hydrogencarbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide; dichloromethane / 0 - 20 °C / Inert atmosphere
2: dichloromethane; diethyl ether / Inert atmosphere
3: mercaptoacetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / Inert atmosphere
With
sodium hydrogencarbonate; benzotriazol-1-ol; mercaptoacetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetonitrile;