triphenylmethyl trimethylsilylethynyl sulfide

Base Information

Chemical Name:triphenylmethyl trimethylsilylethynyl sulfide
CAS No.:950578-38-8
Molecular Formula:C₂₄H₂₄SSi
Molecular Weight:372.606
Hs Code.:

Synonyms:triphenylmethyl trimethylsilylethynyl sulfide

Suppliers and Price of triphenylmethyl trimethylsilylethynyl sulfide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of triphenylmethyl trimethylsilylethynyl sulfide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of triphenylmethyl trimethylsilylethynyl sulfide

There total 1 articles about triphenylmethyl trimethylsilylethynyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 76-83-5
trityl chloride

: 1066-54-2
trimethylsilylacetylene

: 950578-38-8
triphenylmethyl trimethylsilylethynyl sulfide

Guidance literature:: trimethylsilylacetylene; With n-butyllithium; In diethyl ether; hexane; at -78 ℃; for 0.25h;

With sulfur; In diethyl ether; hexane; at -78 - 20 ℃;

trityl chloride; In diethyl ether; hexane; toluene; at 20 ℃; for 12h; Further stages.;
DOI:10.1002/ejoc.200601107

Reference yield: 76.0%

: 950578-38-8
triphenylmethyl trimethylsilylethynyl sulfide

: 950578-40-2
triphenylmethyl ethynyl sulfide

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; methanol; at 20 ℃; for 192h;
DOI:10.1002/ejoc.200601107

Reference yield:

: 950578-38-8
triphenylmethyl trimethylsilylethynyl sulfide

: bis(triphenylmethylthio)acetylene

Guidance literature:: Multi-step reaction with 2 steps

1.1: 76 percent / Bu₄NF / tetrahydrofuran; methanol / 192 h / 20 °C

2.1: LiN(iPr)2 / diethyl ether; tetrahydrofuran / 0.25 h / -78 °C

2.2: S₈ / diethyl ether; tetrahydrofuran / -78 - -40 °C

2.3: 36 percent / diethyl ether; tetrahydrofuran; toluene / -60 - 20 °C

With tetrabutyl ammonium fluoride; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether;
DOI:10.1002/ejoc.200601107