Technology Process of C40H29NO
There total 5 articles about C40H29NO which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
bromotricarbonyl(tetrahydrofuran)rhenium(I) dimer;
In
toluene;
at 115 ℃;
for 24h;
Molecular sieve;
Schlenk technique;
Inert atmosphere;
DOI:10.1021/ol401421r
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tris-(o-tolyl)phosphine; palladium diacetate; triethylamine / acetonitrile / 80 h / 24 °C
2: bromotricarbonyl(tetrahydrofuran)rhenium(I) dimer / toluene / 24 h / 115 °C / Molecular sieve; Schlenk technique; Inert atmosphere
With
bromotricarbonyl(tetrahydrofuran)rhenium(I) dimer; palladium diacetate; triethylamine; tris-(o-tolyl)phosphine;
In
toluene; acetonitrile;
1: |Heck Reaction;
DOI:10.1021/ol401421r
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / 1,4-dioxane; water / 108 °C
2: tris-(o-tolyl)phosphine; palladium diacetate; triethylamine / acetonitrile / 80 h / 24 °C
3: bromotricarbonyl(tetrahydrofuran)rhenium(I) dimer / toluene / 24 h / 115 °C / Molecular sieve; Schlenk technique; Inert atmosphere
With
bromotricarbonyl(tetrahydrofuran)rhenium(I) dimer; palladium diacetate; potassium carbonate; triethylamine; tris-(o-tolyl)phosphine;
In
1,4-dioxane; water; toluene; acetonitrile;
1: |Horner-Wadsworth-Emmons Olefination / 2: |Heck Reaction;
DOI:10.1021/ol401421r
