(2S,3R,4R,5S,6R)-2-(2-(but-3-enyloxy)-4-chloro-5-((5-(furan-2-yl)thiazol-2-yl)methyl)phenyl)-6-(hydroxymethyl)tetrahydro-2H-pyran-3,4,5-triol

Base Information

Chemical Name:(2S,3R,4R,5S,6R)-2-(2-(but-3-enyloxy)-4-chloro-5-((5-(furan-2-yl)thiazol-2-yl)methyl)phenyl)-6-(hydroxymethyl)tetrahydro-2H-pyran-3,4,5-triol
CAS No.:1313513-32-4
Molecular Formula:C₂₄H₂₆ClNO₇S
Molecular Weight:507.992
Hs Code.:

Synonyms:(2S,3R,4R,5S,6R)-2-(2-(but-3-enyloxy)-4-chloro-5-((5-(furan-2-yl)thiazol-2-yl)methyl)phenyl)-6-(hydroxymethyl)tetrahydro-2H-pyran-3,4,5-triol

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Chemical Property of (2S,3R,4R,5S,6R)-2-(2-(but-3-enyloxy)-4-chloro-5-((5-(furan-2-yl)thiazol-2-yl)methyl)phenyl)-6-(hydroxymethyl)tetrahydro-2H-pyran-3,4,5-triol

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Technology Process of (2S,3R,4R,5S,6R)-2-(2-(but-3-enyloxy)-4-chloro-5-((5-(furan-2-yl)thiazol-2-yl)methyl)phenyl)-6-(hydroxymethyl)tetrahydro-2H-pyran-3,4,5-triol

There total 16 articles about (2S,3R,4R,5S,6R)-2-(2-(but-3-enyloxy)-4-chloro-5-((5-(furan-2-yl)thiazol-2-yl)methyl)phenyl)-6-(hydroxymethyl)tetrahydro-2H-pyran-3,4,5-triol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1313513-28-8
(2S,3R,4R,5S,6R)-2-(4-chloro-5-((5-(furan-2-yl)thiazol-2-yl)methyl)-2-hydroxyphenyl)-6-(hydroxymethyl)-tetrahydro-2H-pyran-3,4,5-triol

: 1313513-32-4
(2S,3R,4R,5S,6R)-2-(2-(but-3-enyloxy)-4-chloro-5-((5-(furan-2-yl)thiazol-2-yl)methyl)phenyl)-6-(hydroxymethyl)tetrahydro-2H-pyran-3,4,5-triol

Guidance literature:: With potassium carbonate; In acetone; at 50 ℃; Inert atmosphere;
DOI:10.1016/j.ejmech.2011.03.052

Reference yield:

: 1313513-29-9
5-chloro-4-((5-(furan-2-yl)thiazol-2-yl)methyl)-2-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)-tetrahydro-2H-pyran-2-yl)phenol

: 1313513-32-4
(2S,3R,4R,5S,6R)-2-(2-(but-3-enyloxy)-4-chloro-5-((5-(furan-2-yl)thiazol-2-yl)methyl)phenyl)-6-(hydroxymethyl)tetrahydro-2H-pyran-3,4,5-triol

Guidance literature:: Multi-step reaction with 2 steps

1: boron trichloride / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

2: potassium carbonate / acetone / 50 °C / Inert atmosphere

With boron trichloride; potassium carbonate; In dichloromethane; acetone;
DOI:10.1016/j.ejmech.2011.03.052

Reference yield:

: C₅₁H₅₀ClNO₉

: 1313513-32-4
(2S,3R,4R,5S,6R)-2-(2-(but-3-enyloxy)-4-chloro-5-((5-(furan-2-yl)thiazol-2-yl)methyl)phenyl)-6-(hydroxymethyl)tetrahydro-2H-pyran-3,4,5-triol

Guidance literature:: Multi-step reaction with 4 steps

1: Lawessons reagent / tetrahydrofuran / Inert atmosphere; Reflux

2: sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

3: boron trichloride / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

4: potassium carbonate / acetone / 50 °C / Inert atmosphere

With Lawessons reagent; sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; boron trichloride; potassium carbonate; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1016/j.ejmech.2011.03.052