2-tert-butyl-4-chloro-5-[4-(2-p-toluenesulfonyloxy-d₄-ethoxy-d₂-methyl)benzyl]oxy-3-(2H)-pyridazinone

Base Information

• Chemical Name: 2-tert-butyl-4-chloro-5-[4-(2-p-toluenesulfonyloxy-d₄-ethoxy-d₂-methyl)benzyl]oxy-3-(2H)-pyridazinone
• CAS No.: 1027097-17-1
• Molecular Formula: C₂₅H₂₉ClN₂O₆S
• Molecular Weight: 526.986

Synonyms:2-tert-butyl-4-chloro-5-[4-(2-p-toluenesulfonyloxy-d₄-ethoxy-d₂-methyl)benzyl]oxy-3-(2H)-pyridazinone

Chemical Property of 2-tert-butyl-4-chloro-5-[4-(2-p-toluenesulfonyloxy-d₄-ethoxy-d₂-methyl)benzyl]oxy-3-(2H)-pyridazinone

Chemical Property:

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Technology Process of 2-tert-butyl-4-chloro-5-[4-(2-p-toluenesulfonyloxy-d₄-ethoxy-d₂-methyl)benzyl]oxy-3-(2H)-pyridazinone

There total 1 articles about 2-tert-butyl-4-chloro-5-[4-(2-p-toluenesulfonyloxy-d₄-ethoxy-d₂-methyl)benzyl]oxy-3-(2H)-pyridazinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

2-tert-butyl-4-chloro-5-[4-(2-hydroxy-d4-ethoxy-d2-methyl)benzyloxy]-3-(2H)-pyridazinone (1027097-14-8) + p-toluenesulfonyl chloride (98-59-9) → 2-tert-butyl-4-chloro-5-[4-(2-p-toluenesulfonyloxy-d4-ethoxy-d2-methyl)benzyl]oxy-3-(2H)-pyridazinone (1027097-17-1)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 20 ℃;

DOI:10.1021/jm701443n

Reference yield: 62.0%

2-tert-butyl-4-chloro-5-[4-(2-p-toluenesulfonyloxy-d4-ethoxy-d2-methyl)benzyl]oxy-3-(2H)-pyridazinone (1027097-17-1) → 2-tert-butyl-4-chloro-5-[4-(2-fluoro-d4-ethoxy-d2-methyl)-benzyloxy]-3-(2H)-pyridazinone

Guidance literature:

With potassium fluoride; [2.2.2]cryptande; In acetonitrile; at 90 ℃; for 0.166667h;

DOI:10.1021/jm701443n

Reference yield:

2-tert-butyl-4-chloro-5-[4-(2-p-toluenesulfonyloxy-d4-ethoxy-d2-methyl)benzyl]oxy-3-(2H)-pyridazinone (1027097-17-1) → C18H16(2)H6Cl(18)FN2O3

Guidance literature:

With [¹⁸F]-potassium fluoride; [2.2.2]cryptande; In acetonitrile; at 90 ℃;

DOI:10.1021/jm701443n

upstream raw materials:

2-tert-butyl-4-chloro-5-[4-(2-hydroxy-d₄-ethoxy-d₂-methyl)benzyloxy]-3-(2H)-pyridazinone

p-toluenesulfonyl chloride

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