C₂₈H₃₆N₂O₃Si

Base Information

Chemical Name:C₂₈H₃₆N₂O₃Si
CAS No.:1004985-52-7
Molecular Formula:C₂₈H₃₆N₂O₃Si
Molecular Weight:476.691
Hs Code.:

C<sub>28</sub>H<sub>36</sub>N<sub>2</sub>O<sub>3</sub>Si

Synonyms:C₂₈H₃₆N₂O₃Si

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Chemical Property of C₂₈H₃₆N₂O₃Si

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Technology Process of C₂₈H₃₆N₂O₃Si

There total 9 articles about C₂₈H₃₆N₂O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: C₃₂H₄₄O₆Si

: 1004985-53-8
C₂₈H₃₈O₄Si

: 1004985-52-7
C₂₈H₃₆N₂O₃Si

Guidance literature:: In diethyl ether; at 0 ℃; for 6h;
DOI:10.1002/chem.200700838

Reference yield:

: 20038-12-4
4-bromo-2-methylbut-1-ene

: 1004985-53-8
C₂₈H₃₈O₄Si

: 1004985-52-7
C₂₈H₃₆N₂O₃Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: magnesium / ethylene dibromide; tetrahydrofuran / 1 h / Inert atmosphere; Reflux

1.2: 5 h / -78 °C / Inert atmosphere

2.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

3.1: hydrogenchloride / isopropyl alcohol; water / 2 h / 0 - 20 °C / Inert atmosphere

4.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 2 h / -78 °C / Inert atmosphere

4.2: 2 h / -78 - 20 °C / Inert atmosphere

5.1: magnesium; isopropyl chloride / ethylene dibromide; tetrahydrofuran / 0.5 h / -20 °C / Inert atmosphere

5.2: 1.5 h / -78 °C / Inert atmosphere

6.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C / Inert atmosphere

6.2: 2 h / -78 - 20 °C / Inert atmosphere

7.1: sodium dihydrogen phosphate monohydrate; sodium chlorite / water; tert-butyl alcohol / 0 - 20 °C / Inert atmosphere

8.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

8.2: 2 h / 20 °C / Inert atmosphere

9.1: diethyl ether / 36 h / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; hydrogenchloride; sodium chlorite; sodium dihydrogen phosphate monohydrate; oxalyl dichloride; isopropyl chloride; sodium hydride; magnesium; dimethyl sulfoxide; In tetrahydrofuran; diethyl ether; dichloromethane; water; ethylene dibromide; N,N-dimethyl-formamide; isopropyl alcohol; tert-butyl alcohol; 4.1: |Swern Oxidation / 6.1: |Swern Oxidation;
DOI:10.1002/asia.201403325

Reference yield:

: 1004985-47-0
C₂₄H₃₄O₂Si

: 1004985-53-8
C₂₈H₃₈O₄Si

: 1004985-52-7
C₂₈H₃₆N₂O₃Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 2 h / -78 °C / Inert atmosphere

1.2: 2 h / -78 - 20 °C / Inert atmosphere

2.1: magnesium; isopropyl chloride / ethylene dibromide; tetrahydrofuran / 0.5 h / -20 °C / Inert atmosphere

2.2: 1.5 h / -78 °C / Inert atmosphere

3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C / Inert atmosphere

3.2: 2 h / -78 - 20 °C / Inert atmosphere

4.1: sodium dihydrogen phosphate monohydrate; sodium chlorite / water; tert-butyl alcohol / 0 - 20 °C / Inert atmosphere

5.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

5.2: 2 h / 20 °C / Inert atmosphere

6.1: diethyl ether / 36 h / 0 - 20 °C / Inert atmosphere

With sodium chlorite; sodium dihydrogen phosphate monohydrate; oxalyl dichloride; isopropyl chloride; sodium hydride; magnesium; dimethyl sulfoxide; In tetrahydrofuran; diethyl ether; dichloromethane; water; ethylene dibromide; tert-butyl alcohol; 1.1: |Swern Oxidation / 3.1: |Swern Oxidation;
DOI:10.1002/asia.201403325