2-(3-methyl-4-nitro-phenyl)-thioacetimidic acid 3,3,4,4,4-penta-fluoro-2-oxo-butyl ester

Base Information

Chemical Name:2-(3-methyl-4-nitro-phenyl)-thioacetimidic acid 3,3,4,4,4-penta-fluoro-2-oxo-butyl ester
CAS No.:866639-11-4
Molecular Formula:C₁₃H₁₁F₅N₂O₃S
Molecular Weight:370.3
Hs Code.:

Synonyms:2-(3-methyl-4-nitro-phenyl)-thioacetimidic acid 3,3,4,4,4-penta-fluoro-2-oxo-butyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(3-methyl-4-nitro-phenyl)-thioacetimidic acid 3,3,4,4,4-penta-fluoro-2-oxo-butyl ester

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Technology Process of 2-(3-methyl-4-nitro-phenyl)-thioacetimidic acid 3,3,4,4,4-penta-fluoro-2-oxo-butyl ester

There total 2 articles about 2-(3-methyl-4-nitro-phenyl)-thioacetimidic acid 3,3,4,4,4-penta-fluoro-2-oxo-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 866639-10-3
2-(3-methyl-4-nitro-phenyl)-thioacetamide

: 92737-01-4
1-bromo-3,3,4,4,4-pentafluoro-2-butanone

: 866639-11-4
2-(3-methyl-4-nitro-phenyl)-thioacetimidic acid 3,3,4,4,4-penta-fluoro-2-oxo-butyl ester

Guidance literature:: With potassium carbonate; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 1h;

Reference yield:

: 119713-11-0
(3-methyl-4-nitrophenyl)acetonitrile

: 866639-11-4
2-(3-methyl-4-nitro-phenyl)-thioacetimidic acid 3,3,4,4,4-penta-fluoro-2-oxo-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen sulfide / pyridine / 3 h / 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

With hydrogen sulfide; potassium carbonate; In pyridine; N,N-dimethyl-formamide;